1-[3-(1-cydohexyl-methyl-7-methoxy-1H-indol-3-yl)-[1,2,4]thiadiazol-5-yl]-ethanone

Base Information

Chemical Name:1-[3-(1-cydohexyl-methyl-7-methoxy-1H-indol-3-yl)-[1,2,4]thiadiazol-5-yl]-ethanone
CAS No.:865712-51-2
Molecular Formula:C₂₀H₂₃N₃O₂S
Molecular Weight:369.488
Hs Code.:

Synonyms:1-[3-(1-cydohexyl-methyl-7-methoxy-1H-indol-3-yl)-[1,2,4]thiadiazol-5-yl]-ethanone

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Chemical Property of 1-[3-(1-cydohexyl-methyl-7-methoxy-1H-indol-3-yl)-[1,2,4]thiadiazol-5-yl]-ethanone

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Technology Process of 1-[3-(1-cydohexyl-methyl-7-methoxy-1H-indol-3-yl)-[1,2,4]thiadiazol-5-yl]-ethanone

There total 1 articles about 1-[3-(1-cydohexyl-methyl-7-methoxy-1H-indol-3-yl)-[1,2,4]thiadiazol-5-yl]-ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 865712-48-7
3-(1-cyclohexylmethyl-7-methoxy-1H-indol-3-yl)-[1,2,4]thiadiazole-5-carboxylic acid ethyl ester

: 75-16-1
methylmagnesium bromide

: 865712-51-2
1-[3-(1-cydohexyl-methyl-7-methoxy-1H-indol-3-yl)-[1,2,4]thiadiazol-5-yl]-ethanone

Guidance literature:: 3-(1-cyclohexylmethyl-7-methoxy-1H-indol-3-yl)-[1,2,4]thiadiazole-5-carboxylic acid ethyl ester; methylmagnesium bromide; In diethyl ether; for 0.333333h; Cooling with acetone-dry ice;

With ammonium chloride; In diethyl ether; water; at 20 ℃;

Reference yield:

: 865712-51-2
1-[3-(1-cydohexyl-methyl-7-methoxy-1H-indol-3-yl)-[1,2,4]thiadiazol-5-yl]-ethanone

: 109-89-7
diethylamine

: 1-(cyclohexyl)methyl-3-{5-[1-(diethylamino)ethyl]-[1,2,4]thiadiazol-3-yl}-7-methoxy-1H-indole hydrochloride

Guidance literature:: 1-[3-(1-cydohexyl-methyl-7-methoxy-1H-indol-3-yl)-[1,2,4]thiadiazol-5-yl]-ethanone; diethylamine; With acetic acid; In acetonitrile; for 0.5h;

With polymer supported cyanoborohydride; In acetonitrile; at 150 ℃; for 0.166667h;

With hydrogenchloride; In diethyl ether; dichloromethane;