C₁₃H₁₂N₂OS

Base Information

Chemical Name:C₁₃H₁₂N₂OS
CAS No.:1420830-25-6
Molecular Formula:C₁₃H₁₂N₂OS
Molecular Weight:244.317
Hs Code.:

C<sub>13</sub>H<sub>12</sub>N<sub>2</sub>OS

Synonyms:C₁₃H₁₂N₂OS

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Chemical Property of C₁₃H₁₂N₂OS

Chemical Property:

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Technology Process of C₁₃H₁₂N₂OS

There total 5 articles about C₁₃H₁₂N₂OS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1420830-24-5
C₁₁H₉IN₂OS

: 7486-35-3
tri-n-butyl(vinyl)tin

: 1420830-25-6
C₁₃H₁₂N₂OS

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide; at 90 ℃; for 2h;

Reference yield:

: 1420625-84-8
methyl 3-amino-2-thioformylbut-2-enoate

: 1420830-25-6
C₁₃H₁₂N₂OS

Guidance literature:: Multi-step reaction with 5 steps

1.1: 3-chloro-benzenecarboperoxoic acid / ethanol / 3 h / Reflux

2.1: water; sodium hydroxide / tetrahydrofuran; methanol / 16 h / 40 °C

3.1: n-butyllithium / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

3.2: 1 h / 20 °C

4.1: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 2 h / 20 °C

4.2: 1 h / 20 °C

5.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 2 h / 90 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; oxalyl dichloride; water; N,N-dimethyl-formamide; 3-chloro-benzenecarboperoxoic acid; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 74410-97-2
methyl 3-methylisothiazole-4-carboxylate

: 1420830-25-6
C₁₃H₁₂N₂OS

Guidance literature:: Multi-step reaction with 4 steps

1.1: water; sodium hydroxide / tetrahydrofuran; methanol / 16 h / 40 °C

2.1: n-butyllithium / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

2.2: 1 h / 20 °C

3.1: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 2 h / 20 °C

3.2: 1 h / 20 °C

4.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 2 h / 90 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; oxalyl dichloride; water; N,N-dimethyl-formamide; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;