cis-1-<(thiophenyl)acetyl>-2,3,4,4a,5,6,7,11c-octahydro-5α-chloro-7-<(p-methoxyphenyl)sulfonyl>-1H-pyrido<3,2-c>carbazole

Base Information

Chemical Name:cis-1-<(thiophenyl)acetyl>-2,3,4,4a,5,6,7,11c-octahydro-5α-chloro-7-<(p-methoxyphenyl)sulfonyl>-1H-pyrido<3,2-c>carbazole
CAS No.:88995-71-5
Molecular Formula:C₃₀H₂₉ClN₂O₄S₂
Molecular Weight:581.156
Hs Code.:

Synonyms:cis-1-<(thiophenyl)acetyl>-2,3,4,4a,5,6,7,11c-octahydro-5α-chloro-7-<(p-methoxyphenyl)sulfonyl>-1H-pyrido<3,2-c>carbazole

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Chemical Property of cis-1-<(thiophenyl)acetyl>-2,3,4,4a,5,6,7,11c-octahydro-5α-chloro-7-<(p-methoxyphenyl)sulfonyl>-1H-pyrido<3,2-c>carbazole

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Technology Process of cis-1-<(thiophenyl)acetyl>-2,3,4,4a,5,6,7,11c-octahydro-5α-chloro-7-<(p-methoxyphenyl)sulfonyl>-1H-pyrido<3,2-c>carbazole

There total 4 articles about cis-1-<(thiophenyl)acetyl>-2,3,4,4a,5,6,7,11c-octahydro-5α-chloro-7-<(p-methoxyphenyl)sulfonyl>-1H-pyrido<3,2-c>carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7031-27-8
(phenylthio)acetic acid chloride

: 84960-67-8
cis-2,3,4,4a,5,6,7,11c-octahydro-5α-chloro-7-<(p-methoxyphenyl)-sulfonyl>-1H-pyrido<3,2-c>carbazole

: 88995-71-5
cis-1-<(thiophenyl)acetyl>-2,3,4,4a,5,6,7,11c-octahydro-5α-chloro-7-<(p-methoxyphenyl)sulfonyl>-1H-pyrido<3,2-c>carbazole

Guidance literature:: With sodium hydroxide; In dichloromethane; at 0 ℃; for 0.25h; Yield given;
DOI:10.1021/ja00319a034

Reference yield:

: 80664-26-2
N-<(4-methoxyphenyl)sulfonyl>-2-methylindole-3-carboxaldehyde

: 88995-71-5
cis-1-<(thiophenyl)acetyl>-2,3,4,4a,5,6,7,11c-octahydro-5α-chloro-7-<(p-methoxyphenyl)sulfonyl>-1H-pyrido<3,2-c>carbazole

Guidance literature:: Multi-step reaction with 4 steps

1: 98 percent / 4-Angstroem molecular sieves / CH₂Cl₂ / 15 h

3: 90 percent / zinc, glacial acetic acid / tetrahydrofuran; H₂O / 3 h / 20 °C

4: 1 N NaOH / CH₂Cl₂ / 0.25 h / 0 °C

With sodium hydroxide; 4 A molecular sieve; acetic acid; zinc; In tetrahydrofuran; dichloromethane; water;
DOI:10.1021/ja00319a034

Reference yield:

: 84960-65-6
(E)-1-<(p-methoxyphenyl)sulfonyl>-2-methyl-3-indole

: 88995-71-5
cis-1-<(thiophenyl)acetyl>-2,3,4,4a,5,6,7,11c-octahydro-5α-chloro-7-<(p-methoxyphenyl)sulfonyl>-1H-pyrido<3,2-c>carbazole

Guidance literature:: Multi-step reaction with 3 steps

2: 90 percent / zinc, glacial acetic acid / tetrahydrofuran; H₂O / 3 h / 20 °C

3: 1 N NaOH / CH₂Cl₂ / 0.25 h / 0 °C

With sodium hydroxide; acetic acid; zinc; In tetrahydrofuran; dichloromethane; water;
DOI:10.1021/ja00319a034