(S)-(-)-3-<4-<2-ethoxy>phenyl>-2-ethoxypropanoic acid methyl ester

Base Information

Chemical Name:(S)-(-)-3-<4-<2-ethoxy>phenyl>-2-ethoxypropanoic acid methyl ester
CAS No.:236110-97-7
Molecular Formula:C₂₂H₂₆N₂O₅
Molecular Weight:398.459
Hs Code.:

(S)-(-)-3-<4-<2-<N-(2-benzoxazolyl)-N-methylamino>ethoxy>phenyl>-2-ethoxypropanoic acid methyl ester

Synonyms:(S)-(-)-3-<4-<2-ethoxy>phenyl>-2-ethoxypropanoic acid methyl ester

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Chemical Property of (S)-(-)-3-<4-<2-ethoxy>phenyl>-2-ethoxypropanoic acid methyl ester

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Technology Process of (S)-(-)-3-<4-<2-ethoxy>phenyl>-2-ethoxypropanoic acid methyl ester

There total 2 articles about (S)-(-)-3-<4-<2-ethoxy>phenyl>-2-ethoxypropanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 67-56-1
methanol

: 236110-93-3
<3(2S),4S>-3-<3-<4-<2-ethoxy>phenyl>-2-ethoxypropanoyl>-4-benzyloxazolidin-2-one

: 236110-97-7
(S)-(-)-3-<4-<2-ethoxy>phenyl>-2-ethoxypropanoic acid methyl ester

Guidance literature:: With sodium methylate; at 0 ℃; for 0.333333h;
DOI:10.1016/S0957-4166(99)00112-3

Reference yield:

: 236110-85-3
<3(2S,3R),4S>-3-<3-<4-<2-ethoxy>phenyl>-2-ethoxy-3-hydroxypropanoyl>-4-benzyloxazolidin-2-one

: 236110-97-7
(S)-(-)-3-<4-<2-ethoxy>phenyl>-2-ethoxypropanoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / Et₃SiH, CF₃CO₂H / 60 h / Ambient temperature

2: 86 percent / NaOMe / 0.33 h / 0 °C

With triethylsilane; sodium methylate; trifluoroacetic acid;
DOI:10.1016/S0957-4166(99)00112-3