Technology Process of C28H40N2O2Si
There total 5 articles about C28H40N2O2Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
palladium diacetate; potassium hydrogencarbonate; 2-Biphenylcarboxylic acid;
In
1,2-dichloro-ethane;
at 100 ℃;
for 24h;
regioselective reaction;
DOI:10.1021/ol301214u
- Guidance literature:
-
Multi-step reaction with 4 steps
1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / water; N,N-dimethyl-formamide / 24 h / 20 °C
2: boron tribromide / dichloromethane / 20 °C
3: 1H-imidazole / N,N-dimethyl-formamide / 24 h / 20 °C
4: palladium diacetate; potassium hydrogencarbonate; 2-Biphenylcarboxylic acid / 1,2-dichloro-ethane / 24 h / 100 °C
With
1H-imidazole; palladium diacetate; boron tribromide; benzotriazol-1-ol; potassium hydrogencarbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; 2-Biphenylcarboxylic acid;
In
dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
4: Fujiwara-Moritani reaction;
DOI:10.1021/ol301214u
- Guidance literature:
-
Multi-step reaction with 4 steps
1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / water; N,N-dimethyl-formamide / 24 h / 20 °C
2: boron tribromide / dichloromethane / 20 °C
3: 1H-imidazole / N,N-dimethyl-formamide / 24 h / 20 °C
4: palladium diacetate; potassium hydrogencarbonate; 2-Biphenylcarboxylic acid / 1,2-dichloro-ethane / 24 h / 100 °C
With
1H-imidazole; palladium diacetate; boron tribromide; benzotriazol-1-ol; potassium hydrogencarbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; 2-Biphenylcarboxylic acid;
In
dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
4: Fujiwara-Moritani reaction;
DOI:10.1021/ol301214u
