1-(5-bromo-3-formyl-2-methoxybenzyl)-1H-[1,2,3]triazole-4-carboxylic acid butylamide

Base Information

Chemical Name:1-(5-bromo-3-formyl-2-methoxybenzyl)-1H-[1,2,3]triazole-4-carboxylic acid butylamide
CAS No.:1380204-00-1
Molecular Formula:C₁₆H₁₉BrN₄O₃
Molecular Weight:395.256
Hs Code.:

Synonyms:1-(5-bromo-3-formyl-2-methoxybenzyl)-1H-[1,2,3]triazole-4-carboxylic acid butylamide

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Chemical Property of 1-(5-bromo-3-formyl-2-methoxybenzyl)-1H-[1,2,3]triazole-4-carboxylic acid butylamide

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Technology Process of 1-(5-bromo-3-formyl-2-methoxybenzyl)-1H-[1,2,3]triazole-4-carboxylic acid butylamide

There total 4 articles about 1-(5-bromo-3-formyl-2-methoxybenzyl)-1H-[1,2,3]triazole-4-carboxylic acid butylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1380203-99-5
1-(5-bromo-3-hydroxymethyl-2-methoxybenzyl)-1H-[1,2,3]triazole-4-carboxylic acid butylamide

: 1380204-00-1
1-(5-bromo-3-formyl-2-methoxybenzyl)-1H-[1,2,3]triazole-4-carboxylic acid butylamide

Guidance literature:: With pyridinium chlorochromate; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1039/c2ob25304f

Reference yield:

: 1380203-97-3
(3-azidomethyl-5-bromo-2-methoxyphenyl)methanol

: 1380204-00-1
1-(5-bromo-3-formyl-2-methoxybenzyl)-1H-[1,2,3]triazole-4-carboxylic acid butylamide

Guidance literature:: Multi-step reaction with 3 steps

1: copper(ll) sulfate pentahydrate; sodium ascorbate / ethanol; water / 24 h / 20 °C

2: 4 h / 70 °C

3: pyridinium chlorochromate / dichloromethane / 20 °C / Inert atmosphere

With copper(ll) sulfate pentahydrate; sodium ascorbate; pyridinium chlorochromate; In ethanol; dichloromethane; water;
DOI:10.1039/c2ob25304f

Reference yield:

: 1380203-98-4
1-(5-bromo-3-hydroxymethyl-2-methoxybenzyl)-1H-[1,2,3]triazole-4-carboxylic acid methyl ester

: 1380204-00-1
1-(5-bromo-3-formyl-2-methoxybenzyl)-1H-[1,2,3]triazole-4-carboxylic acid butylamide

Guidance literature:: Multi-step reaction with 2 steps

1: 4 h / 70 °C

2: pyridinium chlorochromate / dichloromethane / 20 °C / Inert atmosphere

With pyridinium chlorochromate; In dichloromethane;
DOI:10.1039/c2ob25304f