Technology Process of C30H35N5O5
There total 6 articles about C30H35N5O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 2,2'-azobis(isobutyronitrile); N-Bromosuccinimide / tetrachloromethane / 72 h / Reflux; Inert atmosphere
2: potassium carbonate; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 20 °C
3: hydrogen / palladium 10% on activated carbon / tetrahydrofuran
4: sodium t-butanolate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / tris-(dibenzylideneacetone)dipalladium(0) / toluene / 110 °C / sealed tube; Inert atmosphere
With
N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); hydrogen; tetra-(n-butyl)ammonium iodide; potassium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate;
tris-(dibenzylideneacetone)dipalladium(0); palladium 10% on activated carbon;
In
tetrahydrofuran; tetrachloromethane; N,N-dimethyl-formamide; toluene;
- Guidance literature:
-
With
2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate;
tris-(dibenzylideneacetone)dipalladium(0);
In
toluene;
at 110 ℃;
sealed tube;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium carbonate / tetrakis(triphenylphosphine) palladium(0) / toluene; 1,2-dimethoxyethane; water / 16 h / 100 °C / Inert atmosphere
2: sodium t-butanolate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / tris-(dibenzylideneacetone)dipalladium(0) / toluene / 110 °C / sealed tube; Inert atmosphere
With
potassium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate;
tris-(dibenzylideneacetone)dipalladium(0); tetrakis(triphenylphosphine) palladium(0);
In
1,2-dimethoxyethane; water; toluene;