[Cu(tris(2-pyridylmethyl)amine)(bis(p-nitrophenylphosphate)](ClO₄)

Base Information

• Chemical Name: [Cu(tris(2-pyridylmethyl)amine)(bis(p-nitrophenylphosphate)](ClO₄)
• CAS No.: 637743-35-2
• Molecular Formula: C₃₀H₂₆CuN₆O₈P*ClO₄
• Molecular Weight: 792.542
• Mol file: 637743-35-2.mol

Synonyms:[Cu(tris(2-pyridylmethyl)amine)(bis(p-nitrophenylphosphate)](ClO₄)

Chemical Property of [Cu(tris(2-pyridylmethyl)amine)(bis(p-nitrophenylphosphate)](ClO₄)

Chemical Property:

Purity/Quality:

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Technology Process of [Cu(tris(2-pyridylmethyl)amine)(bis(p-nitrophenylphosphate)](ClO₄)

There total 1 articles about [Cu(tris(2-pyridylmethyl)amine)(bis(p-nitrophenylphosphate)](ClO₄) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

copper(II) perchlorate hexahydrate + Bis(p-nitrophenyl) phosphate (645-15-8) + tris[(2-pyridylmethyl)amine] (16858-01-8) → [Cu(tris(2-pyridylmethyl)amine)(bis(p-nitrophenylphosphate)](ClO4) (637743-35-2)

Guidance literature:

With NaOH; In methanol; under Ar atm. Cu(ClO4)2*6H2O, TPA, and BNPP were dissolved in MeOH, soln. NaOH in MeOH was added dropwise to pH 6, soln. was warmed to 50°C, DMSO was added dropwise and stirred; soln. was allowed to stand at room temp. overnight;

DOI:10.1021/ic0340985

upstream raw materials:

Bis(p-nitrophenyl) phosphate

tris[(2-pyridylmethyl)amine]