(1S,3'R,4'S,5'R,6'R)-3',4',5'-tris benzyloxy-6'-benzyloxymethyl-5-methylthio-3',4',5',6'-tetrahydro-6-(2-trimethylsilylethynyl)-spiro[isobenzofuro-1(3H),2'-[2H]pyran]

Base Information

Chemical Name:(1S,3'R,4'S,5'R,6'R)-3',4',5'-tris benzyloxy-6'-benzyloxymethyl-5-methylthio-3',4',5',6'-tetrahydro-6-(2-trimethylsilylethynyl)-spiro[isobenzofuro-1(3H),2'-[2H]pyran]
CAS No.:1004780-15-7
Molecular Formula:C₄₇H₅₀O₆SSi
Molecular Weight:771.062
Hs Code.:

(1S,3'R,4'S,5'R,6'R)-3',4',5'-tris benzyloxy-6'-benzyloxymethyl-5-methylthio-3',4',5',6'-tetrahydro-6-(2-trimethylsilylethynyl)-spiro[isobenzofuro-1(3H),2'-[2H]pyran]

Synonyms:(1S,3'R,4'S,5'R,6'R)-3',4',5'-tris benzyloxy-6'-benzyloxymethyl-5-methylthio-3',4',5',6'-tetrahydro-6-(2-trimethylsilylethynyl)-spiro[isobenzofuro-1(3H),2'-[2H]pyran]

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Chemical Property of (1S,3'R,4'S,5'R,6'R)-3',4',5'-tris benzyloxy-6'-benzyloxymethyl-5-methylthio-3',4',5',6'-tetrahydro-6-(2-trimethylsilylethynyl)-spiro[isobenzofuro-1(3H),2'-[2H]pyran]

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Technology Process of (1S,3'R,4'S,5'R,6'R)-3',4',5'-tris benzyloxy-6'-benzyloxymethyl-5-methylthio-3',4',5',6'-tetrahydro-6-(2-trimethylsilylethynyl)-spiro[isobenzofuro-1(3H),2'-[2H]pyran]

There total 1 articles about (1S,3'R,4'S,5'R,6'R)-3',4',5'-tris benzyloxy-6'-benzyloxymethyl-5-methylthio-3',4',5',6'-tetrahydro-6-(2-trimethylsilylethynyl)-spiro[isobenzofuro-1(3H),2'-[2H]pyran] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 75-77-4
chloro-trimethyl-silane

: 1004779-92-3
(1S,3'R,4'S,5'R,6'R)-3',4',5'-tris-benzyloxy-6'-benzyloxymethyl-6-ethynyl-5-methylthio-3',4',5',6'-tetrahydro-spiro[isobenzofuro-1(3H),2'-[2H]pyran]

: 1004780-15-7
(1S,3'R,4'S,5'R,6'R)-3',4',5'-tris benzyloxy-6'-benzyloxymethyl-5-methylthio-3',4',5',6'-tetrahydro-6-(2-trimethylsilylethynyl)-spiro[isobenzofuro-1(3H),2'-[2H]pyran]

Guidance literature:: (1S,3'R,4'S,5'R,6'R)-3',4',5'-tris-benzyloxy-6'-benzyloxymethyl-6-ethynyl-5-methylthio-3',4',5',6'-tetrahydro-spiro[isobenzofuro-1(3H),2'-[2H]pyran]; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1.5h;

chloro-trimethyl-silane; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 1.5h;