7-benzyloxy-6-methoxy-1-(3',4',5'-trimethoxyphenethyl)-N-methyl-3,4-dihydroisoquinolin-2-ium iodide

Base Information

Chemical Name:7-benzyloxy-6-methoxy-1-(3',4',5'-trimethoxyphenethyl)-N-methyl-3,4-dihydroisoquinolin-2-ium iodide
CAS No.:20947-69-7
Molecular Formula:C₂₉H₃₄NO₅*I
Molecular Weight:603.497
Hs Code.:

Synonyms:7-benzyloxy-6-methoxy-1-(3',4',5'-trimethoxyphenethyl)-N-methyl-3,4-dihydroisoquinolin-2-ium iodide

Suppliers and Price of 7-benzyloxy-6-methoxy-1-(3',4',5'-trimethoxyphenethyl)-N-methyl-3,4-dihydroisoquinolin-2-ium iodide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 7-benzyloxy-6-methoxy-1-(3',4',5'-trimethoxyphenethyl)-N-methyl-3,4-dihydroisoquinolin-2-ium iodide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 7-benzyloxy-6-methoxy-1-(3',4',5'-trimethoxyphenethyl)-N-methyl-3,4-dihydroisoquinolin-2-ium iodide

There total 5 articles about 7-benzyloxy-6-methoxy-1-(3',4',5'-trimethoxyphenethyl)-N-methyl-3,4-dihydroisoquinolin-2-ium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67393-37-7
7-benzyloxy-6-methoxy-1-(3',4',5'-trimethoxyphenethyl)-3,4-dihydroisoquinoline

: 74-88-4
methyl iodide

: 20947-69-7
7-benzyloxy-6-methoxy-1-(3',4',5'-trimethoxyphenethyl)-N-methyl-3,4-dihydroisoquinolin-2-ium iodide

Guidance literature:: In ethyl acetate; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.bmcl.2012.04.007

Reference yield:

: 25173-72-2
3-(3,4,5-trimethoxyphenyl)propanoic acid

: 20947-69-7
7-benzyloxy-6-methoxy-1-(3',4',5'-trimethoxyphenethyl)-N-methyl-3,4-dihydroisoquinolin-2-ium iodide

Guidance literature:: Multi-step reaction with 3 steps

1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere

2: trichlorophosphate / acetonitrile / 1 h / Inert atmosphere; Reflux

3: ethyl acetate / 0 - 20 °C / Inert atmosphere

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trichlorophosphate; In ethyl acetate; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.bmcl.2012.04.007

Reference yield:

: 20947-59-5
N-(4-benzyloxy-3-methoxyphenethyl)-3-(3',4',5'-trimethoxyphenyl)propionamide

: 20947-69-7
7-benzyloxy-6-methoxy-1-(3',4',5'-trimethoxyphenethyl)-N-methyl-3,4-dihydroisoquinolin-2-ium iodide

Guidance literature:: Multi-step reaction with 2 steps

1: trichlorophosphate / acetonitrile / 1 h / Inert atmosphere; Reflux

2: ethyl acetate / 0 - 20 °C / Inert atmosphere

With trichlorophosphate; In ethyl acetate; acetonitrile;
DOI:10.1016/j.bmcl.2012.04.007