C₂₃H₂₆N₆O₄

Base Information

Chemical Name:C₂₃H₂₆N₆O₄
CAS No.:1431870-08-4
Molecular Formula:C₂₃H₂₆N₆O₄
Molecular Weight:450.497
Hs Code.:

C<sub>23</sub>H<sub>26</sub>N<sub>6</sub>O<sub>4</sub>

Synonyms:C₂₃H₂₆N₆O₄

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Chemical Property of C₂₃H₂₆N₆O₄

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Technology Process of C₂₃H₂₆N₆O₄

There total 9 articles about C₂₃H₂₆N₆O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

: 930-37-0
glycidyl methyl ether

: 1431873-01-6
C₁₉H₁₈N₆O₂

: 1431870-08-4
C₂₃H₂₆N₆O₄

Guidance literature:: C₁₉H₁₈N₆O₂; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 5 ℃; for 0.75h; Inert atmosphere;

glycidyl methyl ether; In N,N-dimethyl-formamide; mineral oil; at 5 - 80 ℃;

Reference yield:

: 1431872-97-7
C₇H₄BrN₃O

: 1431870-08-4
C₂₃H₂₆N₆O₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / 1,2-dimethoxyethane; water / 100 °C / Inert atmosphere

2.1: N,N-dimethyl-formamide; trichlorophosphate / 1,2-dichloro-ethane / 3 h / 80 °C

3.1: propan-1-ol / 4 h / 100 °C

4.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.75 h / 5 °C / Inert atmosphere

4.2: 5 - 80 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydride; sodium carbonate; N,N-dimethyl-formamide; trichlorophosphate; In propan-1-ol; 1,2-dimethoxyethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 1431872-96-6
C₈H₈ClN₃O₂

: 1431870-08-4
C₂₃H₂₆N₆O₄

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydrogen bromide; acetic acid / 3 h / 40 - 50 °C

2.1: N,N-dimethyl-formamide; trichlorophosphate / 1,2-dichloro-ethane / 3 h / 80 °C

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / 1,2-dimethoxyethane; water / 2 h / Inert atmosphere; Reflux

4.1: propan-1-ol / 4 h / 100 °C

5.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.75 h / 5 °C / Inert atmosphere

5.2: 5 - 80 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; hydrogen bromide; sodium hydride; sodium carbonate; acetic acid; N,N-dimethyl-formamide; trichlorophosphate; In propan-1-ol; 1,2-dimethoxyethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; mineral oil;