Technology Process of C32H40N4O7S
There total 7 articles about C32H40N4O7S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium 10% on activated carbon; hydrazine hydrate;
In
ethanol;
for 2h;
Reflux;
DOI:10.1039/c3ob41209a
- Guidance literature:
-
Multi-step reaction with 7 steps
1: sodium hydroxide / water; tetrahydrofuran / 2 h / 0 °C
2: potassium carbonate / N,N-dimethyl-formamide / 16 h / Reflux
3: triethylamine / dichloromethane / 24 h / 20 °C
4: potassium carbonate / N,N-dimethyl-formamide / 18 h / 85 °C
5: trifluoroacetic acid / dichloromethane / 4 h / 20 °C
6: pyridine / dichloromethane / 2 h / 20 °C
7: hydrazine hydrate; palladium 10% on activated carbon / ethanol / 2 h / Reflux
With
pyridine; palladium 10% on activated carbon; potassium carbonate; hydrazine hydrate; triethylamine; trifluoroacetic acid; sodium hydroxide;
In
tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1039/c3ob41209a
- Guidance literature:
-
Multi-step reaction with 6 steps
1: potassium carbonate / N,N-dimethyl-formamide / 16 h / Reflux
2: triethylamine / dichloromethane / 24 h / 20 °C
3: potassium carbonate / N,N-dimethyl-formamide / 18 h / 85 °C
4: trifluoroacetic acid / dichloromethane / 4 h / 20 °C
5: pyridine / dichloromethane / 2 h / 20 °C
6: hydrazine hydrate; palladium 10% on activated carbon / ethanol / 2 h / Reflux
With
pyridine; palladium 10% on activated carbon; potassium carbonate; hydrazine hydrate; triethylamine; trifluoroacetic acid;
In
ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c3ob41209a
