N¹-{[(methyl)(phenyl)amino](selenocarbonyl)}-4-methyl-N²-phenylbenzimidamide

Base Information

• Chemical Name: N¹-{[(methyl)(phenyl)amino](selenocarbonyl)}-4-methyl-N²-phenylbenzimidamide
• CAS No.: 294644-43-2
• Molecular Formula: C₂₂H₂₁N₃Se
• Molecular Weight: 406.389

Synonyms:N¹-{[(methyl)(phenyl)amino](selenocarbonyl)}-4-methyl-N²-phenylbenzimidamide

Chemical Property of N¹-{[(methyl)(phenyl)amino](selenocarbonyl)}-4-methyl-N²-phenylbenzimidamide

Chemical Property:

Purity/Quality:

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Technology Process of N¹-{[(methyl)(phenyl)amino](selenocarbonyl)}-4-methyl-N²-phenylbenzimidamide

There total 2 articles about N¹-{[(methyl)(phenyl)amino](selenocarbonyl)}-4-methyl-N²-phenylbenzimidamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

N-methylaniline (100-61-8) + 4-methyl-N-phenylbenzimidoyl isoselenocyanate → N1-{[(methyl)(phenyl)amino](selenocarbonyl)}-4-methyl-N2-phenylbenzimidamide (294644-43-2)

Guidance literature:

In acetone; at 25 ℃;

DOI:10.1002/1522-2675(20000705)83:7<1576::AID-HLCA1576>3.0.CO;2-M

Reference yield:

4-methyl-N-phenylbenzamide (6833-18-7) → N1-{[(methyl)(phenyl)amino](selenocarbonyl)}-4-methyl-N2-phenylbenzimidamide (294644-43-2)

Guidance literature:

Multi-step reaction with 3 steps

1: SOCl₂ / 3 h / Heating

2: acetone

3: 85 percent / acetone / 25 °C

With thionyl chloride; In acetone; 1: Substitution / 2: Substitution / 3: Addition;

DOI:10.1002/1522-2675(20000705)83:7<1576::AID-HLCA1576>3.0.CO;2-M

Reference yield: 92.0%

4-cyanobenzyl bromide (17201-43-3) + N1-{[(methyl)(phenyl)amino](selenocarbonyl)}-4-methyl-N2-phenylbenzimidamide (294644-43-2) → N1-{[(4-cyanobenzyl)selanyl][(methyl)(phenyl)amino]methylidene}-4-methyl-N2-phenylbenzimidamide

Guidance literature:

In acetone; at 20 ℃;

DOI:10.1002/1522-2675(20000705)83:7<1576::AID-HLCA1576>3.0.CO;2-M

upstream raw materials:

N-methylaniline

4-methyl-N-phenylbenzamide

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