4-bromo-2-chloro-1-trifluoromethanesulfonyloxybenzene

Base Information

Chemical Name:4-bromo-2-chloro-1-trifluoromethanesulfonyloxybenzene
CAS No.:313510-77-9
Molecular Formula:C₇H₃BrClF₃O₃S
Molecular Weight:339.517
Hs Code.:

Synonyms:4-bromo-2-chloro-1-trifluoromethanesulfonyloxybenzene

Suppliers and Price of 4-bromo-2-chloro-1-trifluoromethanesulfonyloxybenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 4-bromo-2-chloro-1-trifluoromethanesulfonyloxybenzene

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Technology Process of 4-bromo-2-chloro-1-trifluoromethanesulfonyloxybenzene

There total 1 articles about 4-bromo-2-chloro-1-trifluoromethanesulfonyloxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 3964-56-5
4-bromo-2-chlorophenol

: 313510-77-9
4-bromo-2-chloro-1-trifluoromethanesulfonyloxybenzene

Guidance literature:: 4-bromo-2-chlorophenol; With triethylamine; In dichloromethane; at 20 ℃; for 0.0833333h; Inert atmosphere;

trifluoromethylsulfonic anhydride; In dichloromethane; at -78 - 20 ℃; for 12h; Inert atmosphere;
DOI:10.1002/anie.201808386

Reference yield: 90.0%

: 313510-77-9
4-bromo-2-chloro-1-trifluoromethanesulfonyloxybenzene

: 75-08-1
ethanethiol

: 2-chloro-4-(ethylthio)phenyl trifluoromethanesulfonate

Guidance literature:: ethanethiol; With sodium hydride; In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere;

4-bromo-2-chloro-1-trifluoromethanesulfonyloxybenzene; With di-μ-iodobis(tri-t-butylphosphino)dipalladium(l); In tetrahydrofuran; toluene; at 40 ℃; for 12h; chemoselective reaction; Inert atmosphere;
DOI:10.1002/anie.201806036

Reference yield: 86.0%

: 313510-77-9
4-bromo-2-chloro-1-trifluoromethanesulfonyloxybenzene

: 100124-06-9
4-dibenzofurylboronic acid

: 16419-60-6
2-Methylphenylboronic acid

: C₂₆H₁₇F₃O₄S

Guidance literature:: 4-bromo-2-chloro-1-trifluoromethanesulfonyloxybenzene; 2-Methylphenylboronic acid; With potassium fluoride; palladium diacetate; 2-cyclohexyl-3-(diisopropylphosphino)-1-methyl-1H-indole; In tetrahydrofuran; toluene; at 110 ℃; for 2h; Schlenk technique; Inert atmosphere;

4-dibenzofurylboronic acid; In tetrahydrofuran; toluene; at 110 ℃; for 2h; chemoselective reaction;