3-((N-benzylamino)methyl)diisopropylphosphinitobenzene

Base Information

Chemical Name:3-((N-benzylamino)methyl)diisopropylphosphinitobenzene
CAS No.:1233486-94-6
Molecular Formula:C₂₀H₂₈NOP
Molecular Weight:329.422
Hs Code.:

Synonyms:3-((N-benzylamino)methyl)diisopropylphosphinitobenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-((N-benzylamino)methyl)diisopropylphosphinitobenzene

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Technology Process of 3-((N-benzylamino)methyl)diisopropylphosphinitobenzene

There total 1 articles about 3-((N-benzylamino)methyl)diisopropylphosphinitobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 40244-90-4
Chlorodiisopropylphosphane

: 1019483-15-8
3-((N-benzylamino)methyl)phenol

: 1233486-94-6
3-((N-benzylamino)methyl)diisopropylphosphinitobenzene

Guidance literature:: With triethylamine; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ic100914x

Reference yield: 78.0%

: 1233486-94-6
3-((N-benzylamino)methyl)diisopropylphosphinitobenzene

: Br₂Ni*(x)C₂H₃N

: 1233486-86-6
(κP,κC,κN-2,6-(i-Pr2PO)-C6H3-(N-(benzylamino)methyl))NiBr

Guidance literature:: With Et₃N; In toluene; benzene; under N2; soln. of ligand in benzene slowly added to stirred suspn. of Ni compd. and Et3N in toluene at room temp.; heated at 60°C for 3 h; washed with H2O; evapd. to dryness; purified by chromy. (silica gel, hexane, CH2Cl2-hexane 1:1); elem. anal.;
DOI:10.1021/ic100914x

Reference yield:

: 1233486-94-6
3-((N-benzylamino)methyl)diisopropylphosphinitobenzene

: 1233486-90-2
(κP,κC,κN-2-(i-Pr2PO)-6-(CH2N(benzyl)2)C6H3)NiBr

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / benzene; toluene

2: MeLi / toluene

With Et₃N; MeLi; In toluene; benzene;
DOI:10.1021/ic100914x