C₁₈H₂₁N₃O₁₂

Base Information

Chemical Name:C₁₈H₂₁N₃O₁₂
CAS No.:1082706-19-1
Molecular Formula:C₁₈H₂₁N₃O₁₂
Molecular Weight:471.378
Hs Code.:

C<sub>18</sub>H<sub>21</sub>N<sub>3</sub>O<sub>12</sub>

Synonyms:C₁₈H₂₁N₃O₁₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₈H₂₁N₃O₁₂

Chemical Property:

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Technology Process of C₁₈H₂₁N₃O₁₂

There total 5 articles about C₁₈H₂₁N₃O₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1203584-68-2
tert-butyldiphenylsilyl 3,4,6-tri-O-acetyl-2-deoxy-2-(2,4-dinitrophenylamino)-β-D-glucopyranose

: 1082706-19-1
C₁₈H₂₁N₃O₁₂

Guidance literature:: With tetrabutyl ammonium fluoride; acetic acid; In tetrahydrofuran; at 20 ℃; for 1.5h; Inert atmosphere;
DOI:10.1080/07328300903105108

Reference yield:

: 114297-26-6
1,3,4,6-tetra-O-acetyl-2-deoxy-2-{[(4-methoxyphenyl)methylidene]amino}-D-glucopyranose

: 1082706-19-1
C₁₈H₂₁N₃O₁₂

Guidance literature:: Multi-step reaction with 5 steps

1: ammonia / tetrahydrofuran; methanol / 1.5 h / 0 °C

2: 1H-imidazole / dichloromethane / 2 h / 20 °C / Inert atmosphere

3: hydroxylamine hydrochloride / tetrahydrofuran; water / 0.75 h / 20 °C / Inert atmosphere

4: potassium hydrogencarbonate / tetrahydrofuran; water / 6 h / 20 °C / Inert atmosphere

5: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 1.5 h / 20 °C / Inert atmosphere

With 1H-imidazole; hydroxylamine hydrochloride; tetrabutyl ammonium fluoride; ammonia; potassium hydrogencarbonate; acetic acid; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1080/07328300903105108

Reference yield:

: 129729-40-4,130005-73-1
3,4,6-tri-O-acetyl-2-deoxy-2-p-methoxybenzylideneamino-D-glucopyranose

: 1082706-19-1
C₁₈H₂₁N₃O₁₂

Guidance literature:: Multi-step reaction with 4 steps

1: 1H-imidazole / dichloromethane / 2 h / 20 °C / Inert atmosphere

2: hydroxylamine hydrochloride / tetrahydrofuran; water / 0.75 h / 20 °C / Inert atmosphere

3: potassium hydrogencarbonate / tetrahydrofuran; water / 6 h / 20 °C / Inert atmosphere

4: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 1.5 h / 20 °C / Inert atmosphere

With 1H-imidazole; hydroxylamine hydrochloride; tetrabutyl ammonium fluoride; potassium hydrogencarbonate; acetic acid; In tetrahydrofuran; dichloromethane; water;
DOI:10.1080/07328300903105108