tert-butyldiphenylsilyl 3,4,6-tri-O-acetyl-2-deoxy-2-(4-methoxybenzylideneamino)-β-D-glucopyranose

Base Information

Chemical Name:tert-butyldiphenylsilyl 3,4,6-tri-O-acetyl-2-deoxy-2-(4-methoxybenzylideneamino)-β-D-glucopyranose
CAS No.:1203584-53-5
Molecular Formula:C₃₆H₄₃NO₉Si
Molecular Weight:661.824
Hs Code.:

Synonyms:tert-butyldiphenylsilyl 3,4,6-tri-O-acetyl-2-deoxy-2-(4-methoxybenzylideneamino)-β-D-glucopyranose

Suppliers and Price of tert-butyldiphenylsilyl 3,4,6-tri-O-acetyl-2-deoxy-2-(4-methoxybenzylideneamino)-β-D-glucopyranose

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of tert-butyldiphenylsilyl 3,4,6-tri-O-acetyl-2-deoxy-2-(4-methoxybenzylideneamino)-β-D-glucopyranose

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of tert-butyldiphenylsilyl 3,4,6-tri-O-acetyl-2-deoxy-2-(4-methoxybenzylideneamino)-β-D-glucopyranose

There total 2 articles about tert-butyldiphenylsilyl 3,4,6-tri-O-acetyl-2-deoxy-2-(4-methoxybenzylideneamino)-β-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 129729-40-4,130005-73-1
3,4,6-tri-O-acetyl-2-deoxy-2-p-methoxybenzylideneamino-D-glucopyranose

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1203584-53-5
tert-butyldiphenylsilyl 3,4,6-tri-O-acetyl-2-deoxy-2-(4-methoxybenzylideneamino)-β-D-glucopyranose

Guidance literature:: With 1H-imidazole; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1080/07328300903105108

Reference yield:

: 114297-26-6
1,3,4,6-tetra-O-acetyl-2-deoxy-2-{[(4-methoxyphenyl)methylidene]amino}-D-glucopyranose

: 1203584-53-5
tert-butyldiphenylsilyl 3,4,6-tri-O-acetyl-2-deoxy-2-(4-methoxybenzylideneamino)-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: ammonia / tetrahydrofuran; methanol / 1.5 h / 0 °C

2: 1H-imidazole / dichloromethane / 2 h / 20 °C / Inert atmosphere

With 1H-imidazole; ammonia; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1080/07328300903105108

Reference yield: 92.0%

: 1203584-53-5
tert-butyldiphenylsilyl 3,4,6-tri-O-acetyl-2-deoxy-2-(4-methoxybenzylideneamino)-β-D-glucopyranose

: 1203584-54-6
1-O-tert-butyldiphenylsilyl-3,4,6-tri-O-acetyl-2-deoxy-2-amino-β-D-glucopyranoside

Guidance literature:: With hydroxylamine hydrochloride; In tetrahydrofuran; water; at 20 ℃; for 0.75h; Inert atmosphere;
DOI:10.1080/07328300903105108