C₃₄H₃₇N₃O₆

Base Information

• Chemical Name: C₃₄H₃₇N₃O₆
• CAS No.: 1391814-53-1
• Molecular Formula: C₃₄H₃₇N₃O₆
• Molecular Weight: 583.684
• Mol file: 1391814-53-1.mol

Synonyms:C₃₄H₃₇N₃O₆

Chemical Property of C₃₄H₃₇N₃O₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₄H₃₇N₃O₆

There total 5 articles about C₃₄H₃₇N₃O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,6-dibromo-1,4,5,8-naphthalenetetracarboxylic acid dianhydride (83204-68-6) → C34H37N3O6 (1391814-53-1)

Guidance literature:

Multi-step reaction with 4 steps

1.1: potassium carbonate / ethanol

2.1: potassium hydroxide / isopropyl alcohol / 15 h / Reflux

3.1: acetic acid / water / 0.08 h / 160 °C / pH 4 / Microwave irradiation

3.2: 0.5 h / 160 °C

4.1: dichloromethane / 22 h / 20 °C

4.2: 20 h / 55 °C / Molecular sieve

With potassium carbonate; acetic acid; potassium hydroxide; In ethanol; dichloromethane; water; isopropyl alcohol;

DOI:10.1039/c2ob25119a

Reference yield:

C26H30N2O6 (1391814-58-6) + 4-formylphenylboronic acid, (87199-17-5) + isopropylamine (75-31-0) → C34H37N3O6 (1391814-53-1) + C34H37N3O6 (1391814-57-5)

Guidance literature:

C₂₆H₃₀N₂O₆; isopropylamine; In dichloromethane; at 20 ℃; for 22h;

4-formylphenylboronic acid,; With oxygen; copper diacetate; triethylamine; In N,N-dimethyl acetamide; at 55 ℃; for 20h; Molecular sieve;

DOI:10.1039/c2ob25119a

Reference yield:

C18H16O10 (1422618-92-5) → C34H37N3O6 (1391814-53-1)

Guidance literature:

Multi-step reaction with 2 steps

1.1: acetic acid / water / 0.08 h / 160 °C / pH 4 / Microwave irradiation

1.2: 0.5 h / 160 °C

2.1: dichloromethane / 22 h / 20 °C

2.2: 20 h / 55 °C / Molecular sieve

With acetic acid; In dichloromethane; water;

DOI:10.1039/c2ob25119a

upstream raw materials:

tetraethyl 2,6-diethoxynaphthalene-1,4,5,8-tetracarboxylate

C₁₈H₁₆O₁₀

C₂₆H₃₀N₂O₆

4-formylphenylboronic acid,