Technology Process of C28H30ClF2N5O11
There total 9 articles about C28H30ClF2N5O11 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
copper(II) sulfate; sodium L-ascorbate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine;
In
water; dimethyl sulfoxide;
for 8h;
DOI:10.1016/j.bmc.2012.02.001
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: acetic acid; zinc / 1 h / 20 °C
2.1: acetic acid; sodium nitrite / water / 2 h / 0 °C
2.2: 0.5 h / 0 - 20 °C
3.1: 36 h / 20 °C / Inert atmosphere; Neat (no solvent)
3.2: 24 h / 20 °C / Inert atmosphere
4.1: diethylamino-sulfur trifluoride / dichloromethane / 3 h / 20 °C / Inert atmosphere
5.1: sodium methylate / methanol / 2 h / 20 °C / Inert atmosphere
5.2: 20 °C / Inert atmosphere
6.1: sodium hydroxide / water / 1 h / 20 °C
6.2: 20 °C
7.1: copper(II) sulfate; sodium L-ascorbate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine / water; dimethyl sulfoxide / 8 h
With
diethylamino-sulfur trifluoride; sodium methylate; copper(II) sulfate; acetic acid; sodium L-ascorbate; sodium hydroxide; zinc; sodium nitrite; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine;
In
methanol; dichloromethane; water; dimethyl sulfoxide;
DOI:10.1016/j.bmc.2012.02.001
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 36 h / 20 °C / Inert atmosphere; Neat (no solvent)
1.2: 24 h / 20 °C / Inert atmosphere
2.1: diethylamino-sulfur trifluoride / dichloromethane / 3 h / 20 °C / Inert atmosphere
3.1: sodium methylate / methanol / 2 h / 20 °C / Inert atmosphere
3.2: 20 °C / Inert atmosphere
4.1: sodium hydroxide / water / 1 h / 20 °C
4.2: 20 °C
5.1: copper(II) sulfate; sodium L-ascorbate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine / water; dimethyl sulfoxide / 8 h
With
diethylamino-sulfur trifluoride; sodium methylate; copper(II) sulfate; sodium L-ascorbate; sodium hydroxide; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine;
In
methanol; dichloromethane; water; dimethyl sulfoxide;
DOI:10.1016/j.bmc.2012.02.001