(S)-N,N-dibenzyl-2-<1-tert-butyldimethylsilyloxy-4-(1-pyrazolyl)>butylamine

Base Information

Chemical Name:(S)-N,N-dibenzyl-2-<1-tert-butyldimethylsilyloxy-4-(1-pyrazolyl)>butylamine
CAS No.:152299-00-8
Molecular Formula:C₂₇H₃₉N₃OSi
Molecular Weight:449.712
Hs Code.:

Synonyms:(S)-N,N-dibenzyl-2-<1-tert-butyldimethylsilyloxy-4-(1-pyrazolyl)>butylamine

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Chemical Property of (S)-N,N-dibenzyl-2-<1-tert-butyldimethylsilyloxy-4-(1-pyrazolyl)>butylamine

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Technology Process of (S)-N,N-dibenzyl-2-<1-tert-butyldimethylsilyloxy-4-(1-pyrazolyl)>butylamine

There total 6 articles about (S)-N,N-dibenzyl-2-<1-tert-butyldimethylsilyloxy-4-(1-pyrazolyl)>butylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 288-13-1
NH-pyrazole

: 152298-86-7
(S)-1-(3-N,N-dibenzylamino-4-tert-butyldimethylsilyloxy)butylmethanesulfonate

: 152299-00-8
(S)-N,N-dibenzyl-2-<1-tert-butyldimethylsilyloxy-4-(1-pyrazolyl)>butylamine

Guidance literature:: With (Me₃Si)2K; In tetrahydrofuran; toluene; at -20 ℃; for 44h;

Reference yield: 62.0%

: 40802-36-6
potassium pyrazolide

: 152298-86-7
(S)-1-(3-N,N-dibenzylamino-4-tert-butyldimethylsilyloxy)butylmethanesulfonate

: 152299-00-8
(S)-N,N-dibenzyl-2-<1-tert-butyldimethylsilyloxy-4-(1-pyrazolyl)>butylamine

Guidance literature:: In tetrahydrofuran; at 20 ℃; for 40h;
DOI:10.1016/S0040-4039(00)79340-3

Reference yield:

: 161531-12-0
(S)-1-(3-N,N-dibenzylamino-4-hydroxy)butylmethanesulfonate

: 152299-00-8
(S)-N,N-dibenzyl-2-<1-tert-butyldimethylsilyloxy-4-(1-pyrazolyl)>butylamine

Guidance literature:: Multi-step reaction with 2 steps

1: imidazole / dimethylformamide / 1.5 h / -20 °C

2: 62 percent / (Me₃Si)2K / tetrahydrofuran; toluene / 44 h / -20 °C

With 1H-imidazole; (Me₃Si)2K; In tetrahydrofuran; N,N-dimethyl-formamide; toluene;