Phosphorous acid tris-(2,6-diethyl-phenyl) ester

Base Information

Chemical Name:Phosphorous acid tris-(2,6-diethyl-phenyl) ester
CAS No.:100814-85-5
Molecular Formula:C₃₀H₃₉O₃P
Molecular Weight:478.612
Hs Code.:

Synonyms:Phosphorous acid tris-(2,6-diethyl-phenyl) ester

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Chemical Property of Phosphorous acid tris-(2,6-diethyl-phenyl) ester

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Technology Process of Phosphorous acid tris-(2,6-diethyl-phenyl) ester

There total 4 articles about Phosphorous acid tris-(2,6-diethyl-phenyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 1006-59-3
2,6-diethylphenol

: 100814-85-5
Phosphorous acid tris-(2,6-diethyl-phenyl) ester

Guidance literature:: With triethylamine; phosphorus trichloride; In toluene; for 1h; Heating;
DOI:10.1021/ja00270a036

Reference yield:

: 74-85-1
ethene

: 100814-86-6
Phosphorous acid 2,6-diethyl-phenyl ester diphenyl ester

: 100814-82-2
Phosphorous acid bis-(2,6-diethyl-phenyl) ester phenyl ester

: 100814-83-3
Phosphorous acid bis-(2,6-diethyl-phenyl) ester 2-ethyl-phenyl ester

: 100814-85-5
Phosphorous acid tris-(2,6-diethyl-phenyl) ester

Guidance literature:: In toluene; at 194 ℃; for 3.5h; under 4137.2 Torr; Further byproducts given;
DOI:10.1021/ja00270a036

Reference yield:

: 108-95-2,27073-41-2
phenol

: 100814-85-5
Phosphorous acid tris-(2,6-diethyl-phenyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent Chromat_. / <(PhO)3P>4Ru complex, KOPh / tetrahydrofuran / 3.5 h / 177 °C / 4912.9 Torr

2: 54 percent / PCl₃, NEt₃ / toluene / 1 h / Heating

With <(PhO)3P>4Ru; potassium phenolate; triethylamine; phosphorus trichloride; In tetrahydrofuran; toluene;
DOI:10.1021/ja00270a036