2-(4-fluorophenyl)-6-phenylpyridine

Base Information

• Chemical Name: 2-(4-fluorophenyl)-6-phenylpyridine
• CAS No.: 1228437-36-2
• Molecular Formula: C₁₇H₁₂FN
• Molecular Weight: 249.287

Synonyms:2-(4-fluorophenyl)-6-phenylpyridine

Chemical Property of 2-(4-fluorophenyl)-6-phenylpyridine

Chemical Property:

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Technology Process of 2-(4-fluorophenyl)-6-phenylpyridine

There total 14 articles about 2-(4-fluorophenyl)-6-phenylpyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

C17H13FO (296759-67-6,99646-84-1) → 2-(4-fluorophenyl)-6-phenylpyridine (1228437-36-2)

Guidance literature:

With ammonium formate; In toluene; at 110 ℃; for 16h; regioselective reaction;

DOI:10.1055/s-0037-1610725

Reference yield: 82.0%

1-phenylcyclopropan-1-ol (29526-96-3) + 1-(4-fluorophenyl)ethan-1-one-O-acetyl oxime (896885-34-0) → 2-(4-fluorophenyl)-6-phenylpyridine (1228437-36-2)

Guidance literature:

With TEMPOL; In dimethyl sulfoxide; at 120 ℃; chemoselective reaction; Inert atmosphere;

DOI:10.1021/acscatal.9b00832

Reference yield: 81.0%

2-(4-fluorophenyl)pyridine 1-oxide (1262526-01-1) + 5,5-dimethyl-2-phenyl-1,3,2-dioxaborinane (5123-13-7) → 2-(4-fluorophenyl)-6-phenylpyridine (1228437-36-2)

Guidance literature:

With copper acetylacetonate; potassium tert-butylate; oxygen; In toluene; at 110 ℃; for 2h;

DOI:10.1039/c3cc48767a

upstream raw materials:

2-phenylpyridin N-oxide

4-fluorophenylmagnesium chloride

2-(4-fluorophenyl)-5,5-dimethyl-1,3,2-dioxaborinane

2-(4-fluorophenyl)pyridine 1-oxide

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