3-(benzyloxy)-6-(2,5-dimethyl-1H-pyrrol-1-yl)-2-[10-(methoxymethoxy)decyl]-4-methylpyridine

Base Information

Chemical Name:3-(benzyloxy)-6-(2,5-dimethyl-1H-pyrrol-1-yl)-2-[10-(methoxymethoxy)decyl]-4-methylpyridine
CAS No.:1330766-94-3
Molecular Formula:C₃₁H₄₄N₂O₃
Molecular Weight:492.702
Hs Code.:

Synonyms:3-(benzyloxy)-6-(2,5-dimethyl-1H-pyrrol-1-yl)-2-[10-(methoxymethoxy)decyl]-4-methylpyridine

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Chemical Property of 3-(benzyloxy)-6-(2,5-dimethyl-1H-pyrrol-1-yl)-2-[10-(methoxymethoxy)decyl]-4-methylpyridine

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Technology Process of 3-(benzyloxy)-6-(2,5-dimethyl-1H-pyrrol-1-yl)-2-[10-(methoxymethoxy)decyl]-4-methylpyridine

There total 6 articles about 3-(benzyloxy)-6-(2,5-dimethyl-1H-pyrrol-1-yl)-2-[10-(methoxymethoxy)decyl]-4-methylpyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1330766-90-9
3-(benzyloxy)-6-(2,5-dimethyl-1H-pyrrol-1-yl)-2,4-dimethylpyridine

: 317801-83-5
1-bromo-9-(methoxymethoxy)nonane

: 1330766-94-3
3-(benzyloxy)-6-(2,5-dimethyl-1H-pyrrol-1-yl)-2-[10-(methoxymethoxy)decyl]-4-methylpyridine

Guidance literature:: With phenyllithium; In tetrahydrofuran; hexane; at -78 - 23 ℃; for 1h;

Reference yield:

: 5407-87-4
2-Amino-4,6-dimethylpyridine

: 1330766-94-3
3-(benzyloxy)-6-(2,5-dimethyl-1H-pyrrol-1-yl)-2-[10-(methoxymethoxy)decyl]-4-methylpyridine

Guidance literature:: Multi-step reaction with 5 steps

1: N-Bromosuccinimide / acetonitrile / 5 h / 20 °C / Inert atmosphere

2: toluene-4-sulfonic acid / toluene / Reflux; Inert atmosphere

3: potassium hydroxide / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tert-butyl XPhos / 1,4-dioxane; water / 3 h / 100 °C / Inert atmosphere

4: sodium hydride / tetrahydrofuran; mineral oil / 20 °C / Inert atmosphere

5: phenyllithium / hexane; tetrahydrofuran / 1 h / -78 - 23 °C

With N-Bromosuccinimide; sodium hydride; toluene-4-sulfonic acid; phenyllithium; potassium hydroxide; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tert-butyl XPhos; In tetrahydrofuran; 1,4-dioxane; hexane; water; toluene; acetonitrile; mineral oil;

Reference yield:

: 89856-44-0
2-amino-5-bromo-4,6-dimethylpyridine

: 1330766-94-3
3-(benzyloxy)-6-(2,5-dimethyl-1H-pyrrol-1-yl)-2-[10-(methoxymethoxy)decyl]-4-methylpyridine

Guidance literature:: Multi-step reaction with 4 steps

1: toluene-4-sulfonic acid / toluene / Reflux; Inert atmosphere

2: potassium hydroxide / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tert-butyl XPhos / 1,4-dioxane; water / 3 h / 100 °C / Inert atmosphere

3: sodium hydride / tetrahydrofuran; mineral oil / 20 °C / Inert atmosphere

4: phenyllithium / hexane; tetrahydrofuran / 1 h / -78 - 23 °C

With sodium hydride; toluene-4-sulfonic acid; phenyllithium; potassium hydroxide; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tert-butyl XPhos; In tetrahydrofuran; 1,4-dioxane; hexane; water; toluene; mineral oil;