methyl 3-(4-tert-butoxycarbonylpiperazine-1-carbonyl)benzoic acid ester

Base Information

Chemical Name:methyl 3-(4-tert-butoxycarbonylpiperazine-1-carbonyl)benzoic acid ester
CAS No.:1456905-67-1
Molecular Formula:C₁₈H₂₄N₂O₅
Molecular Weight:348.399
Hs Code.:

Synonyms:methyl 3-(4-tert-butoxycarbonylpiperazine-1-carbonyl)benzoic acid ester

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Chemical Property of methyl 3-(4-tert-butoxycarbonylpiperazine-1-carbonyl)benzoic acid ester

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Technology Process of methyl 3-(4-tert-butoxycarbonylpiperazine-1-carbonyl)benzoic acid ester

There total 1 articles about methyl 3-(4-tert-butoxycarbonylpiperazine-1-carbonyl)benzoic acid ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1877-71-0
benzene 1,3-dicarboxylic acid monomethyl ester

: 57260-71-6
1-t-Butoxycarbonylpiperazine

: 1456905-67-1
methyl 3-(4-tert-butoxycarbonylpiperazine-1-carbonyl)benzoic acid ester

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 16h;
DOI:10.1002/anie.201303999

Reference yield: 100.0%

: 1456905-67-1
methyl 3-(4-tert-butoxycarbonylpiperazine-1-carbonyl)benzoic acid ester

: 1395398-39-6
3-(4-tert-butoxycarbonylpiperazine-1-carbonyl)benzoic acid

Guidance literature:: methyl 3-(4-tert-butoxycarbonylpiperazine-1-carbonyl)benzoic acid ester; With lithium hydroxide monohydrate; In methanol; water; at 0 - 20 ℃; for 5h;

With citric acid; In dichloromethane; water; pH=2 - 3;
DOI:10.1002/anie.201303999

Reference yield: 43.0%

: 1456905-67-1
methyl 3-(4-tert-butoxycarbonylpiperazine-1-carbonyl)benzoic acid ester

: 4-((3-chloro-4-ethynylphenoxy)methyl)-5-cyclopropyl-3-(2,6-dichlorophenyl)isoxazole

: tert-butyl 4-(3-((2-chloro-4-((5-cyclopropyl-3-(2,6-dichlorophenyl)isoxazol-4-yl)methoxy)phenyl)ethynyl)-5-(methoxycarbonyl)benzoyl)piperazine-1-carboxylate

Guidance literature:: With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 80 ℃; for 4h;