(4-methoxyphenyl)(4-nitrophenyl)iodonium p-toluenesulfonate

Base Information

• Chemical Name: (4-methoxyphenyl)(4-nitrophenyl)iodonium p-toluenesulfonate
• CAS No.: 1310070-02-0
• Molecular Formula: C₇H₇O₃S*C₁₃H₁₁INO₃
• Molecular Weight: 527.337
• Mol file: 1310070-02-0.mol

Synonyms:(4-methoxyphenyl)(4-nitrophenyl)iodonium p-toluenesulfonate

Chemical Property of (4-methoxyphenyl)(4-nitrophenyl)iodonium p-toluenesulfonate

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (4-methoxyphenyl)(4-nitrophenyl)iodonium p-toluenesulfonate

There total 5 articles about (4-methoxyphenyl)(4-nitrophenyl)iodonium p-toluenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

4-nitrobenzene (73178-10-6) + methoxybenzene (100-66-3) → (4-methoxyphenyl)(4-nitrophenyl)iodonium p-toluenesulfonate (1310070-02-0)

Guidance literature:

In dichloromethane; 2,2,2-trifluoroethanol; at 0 - 20 ℃;

DOI:10.1021/ol2012082

Reference yield: 82.0%

p-nitrobenzene iodide (636-98-6) + toluene-4-sulfonic acid (104-15-4) + methoxybenzene (100-66-3) → (4-methoxyphenyl)(4-nitrophenyl)iodonium p-toluenesulfonate (1310070-02-0)

Guidance literature:

p-nitrobenzene iodide; toluene-4-sulfonic acid; With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃;

methoxybenzene; In dichloromethane; at 20 ℃; for 18h;

DOI:10.1002/chem.202005351

Reference yield: 36.0%

→ (4-methoxyphenyl)(4-nitrophenyl)iodonium p-toluenesulfonate (1310070-02-0)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In chloroform; at 20 ℃; for 0.25h;

In chloroform; at 40 ℃; for 2.5h;

upstream raw materials:

p-nitrobenzene iodide

toluene-4-sulfonic acid

4-nitrobenzene

methoxybenzene

Downstream raw materials:

p-nitrophenylbenzoate

4-[¹²⁵I]iodonitrobenzene

(S)-methyl 2-(4-methoxyphenylamino)-3-phenylpropanoate

4-nitro-N-(3-phenylpropyl)aniline