2-methoxy-6-phenylisonicotinic acid

Base Information

Chemical Name:2-methoxy-6-phenylisonicotinic acid
CAS No.:1041204-92-5
Molecular Formula:C₁₃H₁₁NO₃
Molecular Weight:229.235
Hs Code.:

Synonyms:2-methoxy-6-phenylisonicotinic acid

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Chemical Property of 2-methoxy-6-phenylisonicotinic acid

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Technology Process of 2-methoxy-6-phenylisonicotinic acid

There total 6 articles about 2-methoxy-6-phenylisonicotinic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: methyl 2-methoxy-6-phenylisonicotinate

: 1041204-92-5
2-methoxy-6-phenylisonicotinic acid

Guidance literature:: With lithium hydroxide; In 1,4-dioxane; water; at 20 ℃; for 16h;
DOI:10.1016/j.ejmech.2016.03.020

Reference yield:

: 42521-10-8
2-chloro-6-methoxyisonicotinic acid methyl ester

: 1041204-92-5
2-methoxy-6-phenylisonicotinic acid

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; 1,2-dimethoxyethane / 18 h / 80 °C / Inert atmosphere

2: lithium hydroxide / water; 1,4-dioxane / 16 h / 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; lithium hydroxide; In 1,4-dioxane; 1,2-dimethoxyethane; water; 1: |Suzuki Coupling;
DOI:10.1016/j.ejmech.2016.03.020