IRON, CHLORO[[2,2'-[1,2-ETHANEDIYLBIS[(NITRILO-KN)METHYLIDYNE]]BIS[6-METHOXYPHENOLATO-KO]](2-)]-, (SP-5-13)-

Base Information

Chemical Name:IRON, CHLORO[[2,2'-[1,2-ETHANEDIYLBIS[(NITRILO-KN)METHYLIDYNE]]BIS[6-METHOXYPHENOLATO-KO]](2-)]-, (SP-5-13)-
CAS No.:62945-14-6
Molecular Formula:C₁₈H₁₈FeN₂O₄*Cl
Molecular Weight:417.652
Hs Code.:

Synonyms:Iron,chloro[[2,2'-[1,2-ethanediylbis(nitrilomethylidyne)]bis[6-methoxyphenolato]](2-)-N2,N2',O1,O1']-,(SP-5-13)-; Iron, chloro[a,a'-(ethylenedinitrilo)bis[6-methoxy-o-cresol]ato(2-)]-(7CI); Phenol, 2,2'-[1,2-ethanediylbis(nitrilomethylidyne)]bis[6-methoxy-, ironcomplex; [a,a'-(Ethylenedinitrilo)bis[6-methoxy-o-cresol]ato(2-)]iron chloride

Suppliers and Price of IRON, CHLORO[[2,2'-[1,2-ETHANEDIYLBIS[(NITRILO-KN)METHYLIDYNE]]BIS[6-METHOXYPHENOLATO-KO]](2-)]-, (SP-5-13)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
(SP-5-13)-CHLORO-[[2,2'-[1,2-ETHANEDIYLBIS-[(NITRILO-KN)METHYLIDYNE]]BIS-[6-METHOXYPHENOLATO-KO]](2-)]IRON 95.00%
5MG
$ 504.26

Total 4 raw suppliers

Chemical Property of IRON, CHLORO[[2,2'-[1,2-ETHANEDIYLBIS[(NITRILO-KN)METHYLIDYNE]]BIS[6-METHOXYPHENOLATO-KO]](2-)]-, (SP-5-13)-

Chemical Property:

PSA：61.64000
LogP:2.48620

Purity/Quality:

98%min ^*data from raw suppliers

(SP-5-13)-CHLORO-[[2,2'-[1,2-ETHANEDIYLBIS-[(NITRILO-KN)METHYLIDYNE]]BIS-[6-METHOXYPHENOLATO-KO]](2-)]IRON 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of IRON, CHLORO[[2,2'-[1,2-ETHANEDIYLBIS[(NITRILO-KN)METHYLIDYNE]]BIS[6-METHOXYPHENOLATO-KO]](2-)]-, (SP-5-13)-

There total 2 articles about IRON, CHLORO[[2,2'-[1,2-ETHANEDIYLBIS[(NITRILO-KN)METHYLIDYNE]]BIS[6-METHOXYPHENOLATO-KO]](2-)]-, (SP-5-13)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: iron(III) chloride

: 7396-77-2
N,N'-bis(3-methoxysalicylidene)ethylenediamine

: 62945-14-6
3,3'-dimethoxysalen Fe(III) chloride

Guidance literature:: In methanol; at 60 ℃; for 0.5h;

Reference yield:

: 7396-77-2
N,N'-bis(3-methoxysalicylidene)ethylenediamine

: 7705-08-0
iron(III) chloride

: 62945-14-6
FeCl(1,2-ethylenebis(3-methoxysalicylideneiminate))

Guidance literature:: In ethanol; equimolar amts., room temp., 1 h; collection (filtration), washing (aq. EtOH), drying (vac.), recrystn. (MeOH); elem. anal.;
DOI:10.1039/DT9770000339

Reference yield:

: 288-13-1
NH-pyrazole

: 62945-14-6
Fe(OC₆H₃(OCH₃)CHNCH₂)2Cl(H₂O)

: 143-66-8
sodium tetraphenyl borate

: 95674-15-0
[Fe(OC₆H₃(OCH₃)CHNCH₂)2(C₃H₃N₂H)(H₂O)]⁽¹⁺⁾*B(C₆H₅)4^(1-)*H₂O=[Fe(OC₆H₃(OCH₃)CHNCH₂)2(C₃H₃N₂H)(H₂O)]B(C₆H₅)4*H₂O

Guidance literature:: In methanol; byproducts: [Fe(3-MeO-salen)]2O; complex suspnd. in MeOH, ligand added; soln. refluxed for 10 min; soln. was filtered into a MeOH soln. of NaBPh4, solvent was evapd., ppt. was filtered off, washed with ice-cold MeOH and air dried; elem. anal.;