(R)-5-(benzylthiomethyl)-1-((R)-2-hydroxy-1-phenylethyl)-5-methylimidazolidine-2,4-dione

Base Information

Chemical Name:(R)-5-(benzylthiomethyl)-1-((R)-2-hydroxy-1-phenylethyl)-5-methylimidazolidine-2,4-dione
CAS No.:950672-66-9
Molecular Formula:C₂₀H₂₂N₂O₃S
Molecular Weight:370.472
Hs Code.:

Synonyms:(R)-5-(benzylthiomethyl)-1-((R)-2-hydroxy-1-phenylethyl)-5-methylimidazolidine-2,4-dione

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Chemical Property of (R)-5-(benzylthiomethyl)-1-((R)-2-hydroxy-1-phenylethyl)-5-methylimidazolidine-2,4-dione

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Technology Process of (R)-5-(benzylthiomethyl)-1-((R)-2-hydroxy-1-phenylethyl)-5-methylimidazolidine-2,4-dione

There total 9 articles about (R)-5-(benzylthiomethyl)-1-((R)-2-hydroxy-1-phenylethyl)-5-methylimidazolidine-2,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1367363-42-5
(3R,5R)-methyl 3-(benzylthio-methyl)-3-methyl-2-oxo-5-phenylmorpholine-4-carboxylate

: 950672-66-9
(R)-5-(benzylthiomethyl)-1-((R)-2-hydroxy-1-phenylethyl)-5-methylimidazolidine-2,4-dione

Guidance literature:: With ammonia; In methanol; for 1h; Inert atmosphere; Microwave irradiation;
DOI:10.1016/j.tetlet.2012.02.008

Reference yield: 30.0%

: 1189-71-5
isocyanate de chlorosulfonyle

: 950672-62-5
(R)-3-(benzylthio)-2-methyl-2-((R)-1-phenyl-2-(trimethylsilyloxy)ethylamino)propanenitrile

: 950672-66-9
(R)-5-(benzylthiomethyl)-1-((R)-2-hydroxy-1-phenylethyl)-5-methylimidazolidine-2,4-dione

Guidance literature:: isocyanate de chlorosulfonyle; (R)-3-(benzylthio)-2-methyl-2-((R)-1-phenyl-2-(trimethylsilyloxy)ethylamino)propanenitrile; In dichloromethane; at -55 - 20 ℃; Inert atmosphere;

With hydrogenchloride; In water; for 2h; Inert atmosphere; Reflux;
DOI:10.1016/j.tetlet.2012.02.008

Reference yield:

: 1189-71-5
isocyanate de chlorosulfonyle

: 950672-62-5
(R)-3-(benzylthio)-2-methyl-2-((R)-1-phenyl-2-(trimethylsilyloxy)ethylamino)propanenitrile

: C₂₀H₂₂N₂O₃S₂

: 950672-66-9
(R)-5-(benzylthiomethyl)-1-((R)-2-hydroxy-1-phenylethyl)-5-methylimidazolidine-2,4-dione

: carbamic acid (R)-2-((R)-5-benzylsulfanylmethyl-5-methyl-2,4-dioxo-imidazolidin-1-yl)-2-phenyl-ethyl ester

: C₂₁H₂₃N₃O₄S₂

Guidance literature:: isocyanate de chlorosulfonyle; (R)-3-(benzylthio)-2-methyl-2-((R)-1-phenyl-2-(trimethylsilyloxy)ethylamino)propanenitrile; In dichloromethane; at -55 - 20 ℃; for 2h;

With hydrogenchloride; In water; for 2h; Heating / reflux;