(Z)-1-(4-Chloro-phenyl)-3-{N'-[1-phenyl-prop-(Z)-ylidene]-hydrazino}-but-2-enylideneamine

Base Information

• Chemical Name: (Z)-1-(4-Chloro-phenyl)-3-{N'-[1-phenyl-prop-(Z)-ylidene]-hydrazino}-but-2-enylideneamine
• CAS No.: 90861-51-1
• Molecular Formula: C₁₉H₂₀ClN₃
• Molecular Weight: 325.841

Synonyms:(Z)-1-(4-Chloro-phenyl)-3-{N'-[1-phenyl-prop-(Z)-ylidene]-hydrazino}-but-2-enylideneamine

Chemical Property of (Z)-1-(4-Chloro-phenyl)-3-{N'-[1-phenyl-prop-(Z)-ylidene]-hydrazino}-but-2-enylideneamine

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Technology Process of (Z)-1-(4-Chloro-phenyl)-3-{N'-[1-phenyl-prop-(Z)-ylidene]-hydrazino}-but-2-enylideneamine

There total 1 articles about (Z)-1-(4-Chloro-phenyl)-3-{N'-[1-phenyl-prop-(Z)-ylidene]-hydrazino}-but-2-enylideneamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

4-Cyanochlorobenzene (623-03-0) + N-Isopropylidene-N'-[1-phenyl-prop-(E)-ylidene]-hydrazine (85046-71-5) → (Z)-1-(4-Chloro-phenyl)-3-{N'-[1-phenyl-prop-(Z)-ylidene]-hydrazino}-but-2-enylideneamine (90861-51-1)

Guidance literature:

With lithium diisopropyl amide; In diethyl ether; 1.) 0 deg C, 20 min, 2.) room temperature, 20 h;

Reference yield: 85.0%

(Z)-1-(4-Chloro-phenyl)-3-{N'-[1-phenyl-prop-(Z)-ylidene]-hydrazino}-but-2-enylideneamine (90861-51-1) + dimethyl acetylenedicarboxylate (762-42-5) → 6-(4-Chloro-phenyl)-2-oxo-5-(1-{[1-phenyl-prop-(Z)-ylidene]-hydrazono}-ethyl)-1,2-dihydro-pyridine-4-carboxylic acid methyl ester (113333-65-6)

Guidance literature:

In methanol; for 8h; Ambient temperature;

DOI:10.1055/s-1987-28043

Reference yield: 75.0%

(Z)-1-(4-Chloro-phenyl)-3-{N'-[1-phenyl-prop-(Z)-ylidene]-hydrazino}-but-2-enylideneamine (90861-51-1) → N-[3-(4-Chloro-phenyl)-5-methyl-4,5-dihydro-isoxazol-5-yl]-N'-[1-phenyl-prop-(Z)-ylidene]-hydrazine

Guidance literature:

With pyridine; hydroxylamine hydrochloride; for 6h; Ambient temperature;

upstream raw materials:

4-Cyanochlorobenzene

N-Isopropylidene-N'-[1-phenyl-prop-(E)-ylidene]-hydrazine

Downstream raw materials:

[(E)-1-(4-Chloro-phenyl)-3-{N'-[1-phenyl-prop-(E)-ylidene]-hydrazino}-but-2-en-(Z)-ylidene]-carbamic acid ethyl ester

(E)-2-Chloro-1-(4-chloro-phenyl)-3-{N'-[1-phenyl-prop-(Z)-ylidene]-hydrazino}-but-2-enylideneamine

4-(4-Chloro-phenyl)-6-methyl-1-[1-phenyl-prop-(E)-ylideneamino]-1H-pyrimidin-2-one

6-(4-Chloro-phenyl)-2-oxo-5-(1-{[1-phenyl-prop-(Z)-ylidene]-hydrazono}-ethyl)-1,2-dihydro-pyridine-4-carboxylic acid methyl ester

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