(S)-5-tert-Butoxycarbonylamino-2-[methyl-(toluene-4-sulfonyl)-amino]-pentanoic acid; compound with dicyclohexyl-amine

Base Information

Chemical Name:(S)-5-tert-Butoxycarbonylamino-2-[methyl-(toluene-4-sulfonyl)-amino]-pentanoic acid; compound with dicyclohexyl-amine
CAS No.:124312-57-8
Molecular Formula:C₁₂H₂₃N*C₁₈H₂₈N₂O₆S
Molecular Weight:581.817
Hs Code.:

Synonyms:(S)-5-tert-Butoxycarbonylamino-2-[methyl-(toluene-4-sulfonyl)-amino]-pentanoic acid; compound with dicyclohexyl-amine

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Chemical Property of (S)-5-tert-Butoxycarbonylamino-2-[methyl-(toluene-4-sulfonyl)-amino]-pentanoic acid; compound with dicyclohexyl-amine

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Technology Process of (S)-5-tert-Butoxycarbonylamino-2-[methyl-(toluene-4-sulfonyl)-amino]-pentanoic acid; compound with dicyclohexyl-amine

There total 2 articles about (S)-5-tert-Butoxycarbonylamino-2-[methyl-(toluene-4-sulfonyl)-amino]-pentanoic acid; compound with dicyclohexyl-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 124312-52-3
(S)-5-Acetylamino-2-[methyl-(toluene-4-sulfonyl)-amino]-pentanoic acid isopropyl ester

: 101-83-7
N-cyclohexyl-cyclohexanamine

: 124312-57-8
(S)-5-tert-Butoxycarbonylamino-2-[methyl-(toluene-4-sulfonyl)-amino]-pentanoic acid; compound with dicyclohexyl-amine

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; water; for 4h; Heating;

Reference yield:

: 34605-48-6
N^α-Acetyl-N^α-tosyl-L-ornithine-isopropylester

: 124312-57-8
(S)-5-tert-Butoxycarbonylamino-2-[methyl-(toluene-4-sulfonyl)-amino]-pentanoic acid; compound with dicyclohexyl-amine

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / NaOH / H₂O / 4 h / Ambient temperature; detergent

2: 88 percent / HCl / H₂O; dioxane / 4 h / Heating

With hydrogenchloride; sodium hydroxide; In 1,4-dioxane; water;

Reference yield: 73.0%

: 593-51-1
methylamine hydrochloride

: 124312-57-8
(S)-5-tert-Butoxycarbonylamino-2-[methyl-(toluene-4-sulfonyl)-amino]-pentanoic acid; compound with dicyclohexyl-amine

: 124337-32-2
{(S)-4-Methylcarbamoyl-4-[methyl-(toluene-4-sulfonyl)-amino]-butyl}-carbamic acid tert-butyl ester

Guidance literature:: With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; 1. -12 deg C, 30 min; 2. 0 deg C, 2 h; 3. 5 deg c, 18 h;