N,N,N-trimethyl-1-(4-(trifluoromethyl)phenyl)methanaminium trifluoromethanesulfonate

Base Information

Chemical Name:N,N,N-trimethyl-1-(4-(trifluoromethyl)phenyl)methanaminium trifluoromethanesulfonate
CAS No.:1416982-09-6
Molecular Formula:CF₃O₃S*C₁₁H₁₅F₃N
Molecular Weight:367.312
Hs Code.:

Synonyms:N,N,N-trimethyl-1-(4-(trifluoromethyl)phenyl)methanaminium trifluoromethanesulfonate

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Chemical Property of N,N,N-trimethyl-1-(4-(trifluoromethyl)phenyl)methanaminium trifluoromethanesulfonate

Chemical Property:

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Technology Process of N,N,N-trimethyl-1-(4-(trifluoromethyl)phenyl)methanaminium trifluoromethanesulfonate

There total 2 articles about N,N,N-trimethyl-1-(4-(trifluoromethyl)phenyl)methanaminium trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 71740-33-5
N,N-dimethyl-1-(4-(trifluoromethyl)phenyl)methanamine

: 333-27-7
methyl trifluoromethanesulfonate

: 1416982-09-6
N,N,N-trimethyl-1-(4-(trifluoromethyl)phenyl)methanaminium trifluoromethanesulfonate

Guidance literature:: In diethyl ether; at 0 ℃; for 0.25h;
DOI:10.1021/ja3089422

Reference yield:

: 455-19-6
4-Trifluoromethylbenzaldehyde

: 1416982-09-6
N,N,N-trimethyl-1-(4-(trifluoromethyl)phenyl)methanaminium trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: titanium(IV) isopropylate / methanol / 20 °C

1.2: 1.5 h / 20 °C

2.1: diethyl ether / 2.25 h / 0 - 20 °C

With titanium(IV) isopropylate; In methanol; diethyl ether;
DOI:10.1021/jacs.9b05224

Reference yield: 100.0%

: 1416982-09-6
N,N,N-trimethyl-1-(4-(trifluoromethyl)phenyl)methanaminium trifluoromethanesulfonate

: 5720-05-8
4-methylphenylboronic acid

: 170789-13-6
1-methyl-4-(4-(trifluoromethyl)benzyl)benzene

Guidance literature:: With bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; potassium phosphate; cyclohexyldiphenylphosphine; In 1,4-dioxane; at 40 ℃; for 24h; Reagent/catalyst; Inert atmosphere; Glovebox;
DOI:10.1021/ja3089422