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dimesitylmethoxygermane

Base Information
  • Chemical Name:dimesitylmethoxygermane
  • CAS No.:131368-48-4
  • Molecular Formula:C19H26GeO
  • Molecular Weight:343.005
  • Hs Code.:
dimesitylmethoxygermane

Synonyms:dimesitylmethoxygermane

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Chemical Property of dimesitylmethoxygermane
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Technology Process of dimesitylmethoxygermane

There total 4 articles about dimesitylmethoxygermane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
In Cyclohexane-d12; byproducts: 2,3-dimethyl-1,3-butadiene; Irradiation (UV/VIS); photolysis of a soln. of germanium compd. in C6D12 with methanol at 254 nm;
DOI:10.1021/ja046308y
Guidance literature:
With methanol; In tetrahydrofuran; byproducts: N2; under Ar or N2, 50°C for 3 h; identified by (1)H-NMR;
DOI:10.1016/0022-328X(90)85307-K
Guidance literature:
In tetrahydrofuran; byproducts: Si2(CH3)6, C6H3(CH3)3, (CH3)3SiC6H2(CH3)3; Irradiation (UV/VIS); (Ar); photolysis of THF soln. of germanium compd. at -70°C for 24h, addn. of methanol prior to exposure to air; warming to room temp., evapn., thin layer chromy. (silica gel, hexanes),NMR and MAS;
DOI:10.1139/V07-039
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