Technology Process of C39H46FNO7
There total 5 articles about C39H46FNO7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C31H31FO7;
With
caesium carbonate;
In
acetone;
at 0 ℃;
for 0.166667h;
(R)-1-((S)-2-chloro-1-methyl-ethyl)-3-methyl-pyrrolidine hydrochloride;
In
acetone;
at 60 ℃;
for 19h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: boron tribromide / dichloromethane / -30 - 25 °C
2.1: boron trifluoride diethyl etherate / 0.25 h / Reflux
3.1: hydrogenchloride / 0.75 h / -10 - 0 °C
4.1: piperidine / benzene / 16 h / Dean-Stark; Reflux
5.1: caesium carbonate / acetone / 0.17 h / 0 °C
5.2: 19 h / 60 °C
With
piperidine; hydrogenchloride; boron trifluoride diethyl etherate; boron tribromide; caesium carbonate;
In
dichloromethane; acetone; benzene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: boron trifluoride diethyl etherate / 0.25 h / Reflux
2.1: hydrogenchloride / 0.75 h / -10 - 0 °C
3.1: piperidine / benzene / 16 h / Dean-Stark; Reflux
4.1: caesium carbonate / acetone / 0.17 h / 0 °C
4.2: 19 h / 60 °C
With
piperidine; hydrogenchloride; boron trifluoride diethyl etherate; caesium carbonate;
In
acetone; benzene;