{3-[3-(2-azido-phenyl)-1-methyl-propa-1,2-dienyl]-6,6-dimethyl-cyclohex-2-enyloxy}-tert-butyl-dimethyl-silane

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Chemical Name:{3-[3-(2-azido-phenyl)-1-methyl-propa-1,2-dienyl]-6,6-dimethyl-cyclohex-2-enyloxy}-tert-butyl-dimethyl-silane
CAS No.:1020202-67-8
Molecular Formula:C₂₄H₃₅N₃OSi
Molecular Weight:409.647
Hs Code.:

Synonyms:{3-[3-(2-azido-phenyl)-1-methyl-propa-1,2-dienyl]-6,6-dimethyl-cyclohex-2-enyloxy}-tert-butyl-dimethyl-silane

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Chemical Property of {3-[3-(2-azido-phenyl)-1-methyl-propa-1,2-dienyl]-6,6-dimethyl-cyclohex-2-enyloxy}-tert-butyl-dimethyl-silane

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Technology Process of {3-[3-(2-azido-phenyl)-1-methyl-propa-1,2-dienyl]-6,6-dimethyl-cyclohex-2-enyloxy}-tert-butyl-dimethyl-silane

There total 1 articles about {3-[3-(2-azido-phenyl)-1-methyl-propa-1,2-dienyl]-6,6-dimethyl-cyclohex-2-enyloxy}-tert-butyl-dimethyl-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1020202-66-7
1-(2-azido-phenyl)-3-[3-(tert-butyldimethylsilanyloxy)-4,4-dimethyl-cyclohex-1-enyl]-prop-2-ynyl acetate

: 75-16-1
methylmagnesium bromide

: 1020202-67-8
{3-[3-(2-azido-phenyl)-1-methyl-propa-1,2-dienyl]-6,6-dimethyl-cyclohex-2-enyloxy}-tert-butyl-dimethyl-silane

Guidance literature:: methylmagnesium bromide; With copper(l) iodide; lithium bromide; In tetrahydrofuran; diethyl ether; for 0.5h; Cooling with ice;

1-(2-azido-phenyl)-3-[3-(tert-butyldimethylsilanyloxy)-4,4-dimethyl-cyclohex-1-enyl]-prop-2-ynyl acetate; In tetrahydrofuran; diethyl ether; for 0.5h; Cooling with ice;

With water; ammonium chloride; In tetrahydrofuran; diethyl ether; Cooling with ice;
DOI:10.1021/ol800429j