6-(tert-butyl) 7-methyl 4-((benzyloxy)amino)-2-trityl-2,4,5,7-tetrahydro-6H-pyrazolo[3,4-c]pyridine-6,7-dicarboxylate

Base Information

Chemical Name:6-(tert-butyl) 7-methyl 4-((benzyloxy)amino)-2-trityl-2,4,5,7-tetrahydro-6H-pyrazolo[3,4-c]pyridine-6,7-dicarboxylate
CAS No.:478628-00-1
Molecular Formula:C₃₉H₄₀N₄O₅
Molecular Weight:644.77
Hs Code.:

Synonyms:6-(tert-butyl) 7-methyl 4-((benzyloxy)amino)-2-trityl-2,4,5,7-tetrahydro-6H-pyrazolo[3,4-c]pyridine-6,7-dicarboxylate

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Chemical Property of 6-(tert-butyl) 7-methyl 4-((benzyloxy)amino)-2-trityl-2,4,5,7-tetrahydro-6H-pyrazolo[3,4-c]pyridine-6,7-dicarboxylate

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Technology Process of 6-(tert-butyl) 7-methyl 4-((benzyloxy)amino)-2-trityl-2,4,5,7-tetrahydro-6H-pyrazolo[3,4-c]pyridine-6,7-dicarboxylate

There total 10 articles about 6-(tert-butyl) 7-methyl 4-((benzyloxy)amino)-2-trityl-2,4,5,7-tetrahydro-6H-pyrazolo[3,4-c]pyridine-6,7-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 478627-99-5
6-(tert-butyl) 7-methyl 4-hydroxy-2-trityl-2,4,5,7-tetrahydro-6H-pyrazolo[3,4-c]pyridine-6,7-dicarboxylate

: 7143-01-3
Methanesulfonic anhydride

: 478628-00-1
6-(tert-butyl) 7-methyl 4-((benzyloxy)amino)-2-trityl-2,4,5,7-tetrahydro-6H-pyrazolo[3,4-c]pyridine-6,7-dicarboxylate

Guidance literature:: With triethylamine; In dichloromethane; at -70 ℃; for 1h;

Reference yield: 58.6%

: 478627-99-5
6-(tert-butyl) 7-methyl 4-hydroxy-2-trityl-2,4,5,7-tetrahydro-6H-pyrazolo[3,4-c]pyridine-6,7-dicarboxylate

: 622-33-3
N-benzyloxyamine

: 478628-00-1
6-(tert-butyl) 7-methyl 4-((benzyloxy)amino)-2-trityl-2,4,5,7-tetrahydro-6H-pyrazolo[3,4-c]pyridine-6,7-dicarboxylate

Guidance literature:: 6-(tert-butyl) 7-methyl 4-hydroxy-2-trityl-2,4,5,7-tetrahydro-6H-pyrazolo[3,4-c]pyridine-6,7-dicarboxylate; With triethylamine; Methanesulfonic anhydride; In dichloromethane; at -60 ℃; for 2.5h; Inert atmosphere;

N-benzyloxyamine; In dichloromethane; at -60 - 20 ℃; Inert atmosphere;