12-benzoyloxy-7,8-dimethoxy-2,3-methylenedioxy-6-trifluoromethanesulfonyloxybenzo[c]phenanthridine

Base Information

Chemical Name:12-benzoyloxy-7,8-dimethoxy-2,3-methylenedioxy-6-trifluoromethanesulfonyloxybenzo[c]phenanthridine
CAS No.:628328-83-6
Molecular Formula:C₂₈H₁₈F₃NO₉S
Molecular Weight:601.513
Hs Code.:

Synonyms:12-benzoyloxy-7,8-dimethoxy-2,3-methylenedioxy-6-trifluoromethanesulfonyloxybenzo[c]phenanthridine

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Chemical Property of 12-benzoyloxy-7,8-dimethoxy-2,3-methylenedioxy-6-trifluoromethanesulfonyloxybenzo[c]phenanthridine

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Technology Process of 12-benzoyloxy-7,8-dimethoxy-2,3-methylenedioxy-6-trifluoromethanesulfonyloxybenzo[c]phenanthridine

There total 6 articles about 12-benzoyloxy-7,8-dimethoxy-2,3-methylenedioxy-6-trifluoromethanesulfonyloxybenzo[c]phenanthridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 628328-82-5
12-benzoyloxy-7,8-dimethoxy-2,3-methylenedioxybenzo[c]phenanthridin-6(5H)-one

: 628328-83-6
12-benzoyloxy-7,8-dimethoxy-2,3-methylenedioxy-6-trifluoromethanesulfonyloxybenzo[c]phenanthridine

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 ℃; for 5h;
DOI:10.1039/b304216m

Reference yield:

: 628328-74-5
methyl 6-[3-(1-benzyloxy-6,7-methylenedioxynaphthyl)]-2,3-dimethoxybenzoate

: 628328-83-6
12-benzoyloxy-7,8-dimethoxy-2,3-methylenedioxy-6-trifluoromethanesulfonyloxybenzo[c]phenanthridine

Guidance literature:: Multi-step reaction with 6 steps

1: 82 percent / H₂; aq. HCl / Pd/C / acetic acid / 3.5 h / 20 °C

2: K₂CO₃; i-C₅H₁₁ONO / dimethylformamide / 3.5 h / 20 °C

3: 336 mg / dimethylformamide / 1.5 h / 20 °C

4: 95 percent / H₂ / 10percent Pd/C / acetic acid / 1.5 h / 20 °C

5: 96 percent / CH₂Cl₂ / 336 h / 60 °C

6: 83 percent / diisopropylethylamine / CH₂Cl₂ / 5 h / 0 °C

With hydrogenchloride; hydrogen; potassium carbonate; N-ethyl-N,N-diisopropylamine; isopentyl nitrite; palladium on activated charcoal; In dichloromethane; acetic acid; N,N-dimethyl-formamide;
DOI:10.1039/b304216m

Reference yield:

: 628328-75-6
methyl 6-[3-(1-hydroxy-6,7-methylenedioxynaphthyl)]-2,3-dimethoxybenzoate

: 628328-83-6
12-benzoyloxy-7,8-dimethoxy-2,3-methylenedioxy-6-trifluoromethanesulfonyloxybenzo[c]phenanthridine

Guidance literature:: Multi-step reaction with 5 steps

1: K₂CO₃; i-C₅H₁₁ONO / dimethylformamide / 3.5 h / 20 °C

2: 336 mg / dimethylformamide / 1.5 h / 20 °C

3: 95 percent / H₂ / 10percent Pd/C / acetic acid / 1.5 h / 20 °C

4: 96 percent / CH₂Cl₂ / 336 h / 60 °C

5: 83 percent / diisopropylethylamine / CH₂Cl₂ / 5 h / 0 °C

With hydrogen; potassium carbonate; N-ethyl-N,N-diisopropylamine; isopentyl nitrite; 10percent Pd/C; In dichloromethane; acetic acid; N,N-dimethyl-formamide;
DOI:10.1039/b304216m