methyl 6-[3-(1-hydroxy-6,7-methylenedioxynaphthyl)]-2,3-dimethoxybenzoate

Base Information

Chemical Name:methyl 6-[3-(1-hydroxy-6,7-methylenedioxynaphthyl)]-2,3-dimethoxybenzoate
CAS No.:628328-75-6
Molecular Formula:C₂₁H₁₈O₇
Molecular Weight:382.37
Hs Code.:

Synonyms:methyl 6-[3-(1-hydroxy-6,7-methylenedioxynaphthyl)]-2,3-dimethoxybenzoate

Suppliers and Price of methyl 6-[3-(1-hydroxy-6,7-methylenedioxynaphthyl)]-2,3-dimethoxybenzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 2 raw suppliers

Chemical Property of methyl 6-[3-(1-hydroxy-6,7-methylenedioxynaphthyl)]-2,3-dimethoxybenzoate

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of methyl 6-[3-(1-hydroxy-6,7-methylenedioxynaphthyl)]-2,3-dimethoxybenzoate

There total 6 articles about methyl 6-[3-(1-hydroxy-6,7-methylenedioxynaphthyl)]-2,3-dimethoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 628328-74-5
methyl 6-[3-(1-benzyloxy-6,7-methylenedioxynaphthyl)]-2,3-dimethoxybenzoate

: 628328-75-6
methyl 6-[3-(1-hydroxy-6,7-methylenedioxynaphthyl)]-2,3-dimethoxybenzoate

Guidance literature:: With hydrogenchloride; hydrogen; palladium on activated charcoal; In acetic acid; at 20 ℃; for 3.5h;
DOI:10.1039/b304216m

Reference yield: 15.0%

: methyl 6-(5,8-dihydro-5,8-epoxynaphtho[2,3-d][1,3]dioxol-6-yl)-2,3-dimethoxybenzoate

: 1,2-dimethoxy-13H-[1,3]dioxolo[4',5':4,5]benzo[1,2-h]benzo[c]chromene-13-one

: 628328-75-6
methyl 6-[3-(1-hydroxy-6,7-methylenedioxynaphthyl)]-2,3-dimethoxybenzoate

Guidance literature:: With toluene-4-sulfonic acid; In methanol;
DOI:10.1021/acs.joc.5b00107

Reference yield:

: 6941-70-4
2-bromo-4,5-methylenedioxyphenol

: 1,2-dimethoxy-13H-[1,3]dioxolo[4',5':4,5]benzo[1,2-h]benzo[c]chromene-13-one

: 628328-75-6
methyl 6-[3-(1-hydroxy-6,7-methylenedioxynaphthyl)]-2,3-dimethoxybenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: n-butyllithium

2: cesium fluoride / acetonitrile / 24 h / 23 °C / Inert atmosphere

3: toluene-4-sulfonic acid / methanol

With n-butyllithium; toluene-4-sulfonic acid; cesium fluoride; In methanol; acetonitrile;
DOI:10.1021/acs.joc.5b00107