N-(2-(3,4,5-tris(dodecyloxy)benzamido)ethyl)-5-bromothiophene-2-carboxamide

Base Information

Chemical Name:N-(2-(3,4,5-tris(dodecyloxy)benzamido)ethyl)-5-bromothiophene-2-carboxamide
CAS No.:1304141-95-4
Molecular Formula:C₅₀H₈₅BrN₂O₅S
Molecular Weight:906.205
Hs Code.:

Synonyms:N-(2-(3,4,5-tris(dodecyloxy)benzamido)ethyl)-5-bromothiophene-2-carboxamide

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Chemical Property of N-(2-(3,4,5-tris(dodecyloxy)benzamido)ethyl)-5-bromothiophene-2-carboxamide

Chemical Property:

Purity/Quality:

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Technology Process of N-(2-(3,4,5-tris(dodecyloxy)benzamido)ethyl)-5-bromothiophene-2-carboxamide

There total 6 articles about N-(2-(3,4,5-tris(dodecyloxy)benzamido)ethyl)-5-bromothiophene-2-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 912275-84-4
N-(2-aminoethyl)-3,4,5-tris(dodecyloxy)benzamide

: 7311-63-9
5-bromothiophene-2-carboxylic acid

: 1304141-95-4
N-(2-(3,4,5-tris(dodecyloxy)benzamido)ethyl)-5-bromothiophene-2-carboxamide

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃;
DOI:10.1039/c1cc10809c

Reference yield:

: 1304141-92-1
tert-butyl 2-(3,4,5-tris(dodecyloxy)benzamido)ethylcarbamate

: 1304141-95-4
N-(2-(3,4,5-tris(dodecyloxy)benzamido)ethyl)-5-bromothiophene-2-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / 1,4-dioxane; ethyl acetate / 2 h

2: ; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C

With hydrogenchloride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In 1,4-dioxane; dichloromethane; ethyl acetate;
DOI:10.1039/c1cc10809c

Reference yield:

: 99-24-1
methyl galloate

: 1304141-95-4
N-(2-(3,4,5-tris(dodecyloxy)benzamido)ethyl)-5-bromothiophene-2-carboxamide

Guidance literature:: Multi-step reaction with 5 steps

1: 18-crown-6 ether; potassium carbonate / acetone / Reflux

2: water; sodium hydroxide / tetrahydrofuran; methanol / 16 h / Reflux

3: ; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C

4: hydrogenchloride / 1,4-dioxane; ethyl acetate / 2 h

5: ; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C

With hydrogenchloride; 18-crown-6 ether; water; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; ethyl acetate; acetone;
DOI:10.1039/c1cc10809c