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O-acetyltartronic acid dimethyl ester

Base Information
  • Chemical Name:O-acetyltartronic acid dimethyl ester
  • CAS No.:32786-27-9
  • Molecular Formula:C7H10O6
  • Molecular Weight:190.153
  • Hs Code.:
O-acetyltartronic acid dimethyl ester

Synonyms:O-acetyltartronic acid dimethyl ester

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Chemical Property of O-acetyltartronic acid dimethyl ester
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Technology Process of O-acetyltartronic acid dimethyl ester

There total 1 articles about O-acetyltartronic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With chromium(VI) oxide; hydrogenchloride; acetic anhydride; acetyl chloride; Product distribution; multistep reaction: 1.) 20 deg C, 30 min, 2.) reflux, 0.5 h; CrO3 oxidation of anomeric methyl galactopyranosides, effect of the anomeric centre confuguration on the rate of oxidation; effect of the temperature and time on the degree of oxidation;
DOI:10.1007/BF00961769
Guidance literature:
With Methyl-4,6-O-benzylidene-2,3-dideoxy-α-D-glucopyranosido[2,3-h]-N-3-hydroxypropyl-1,4,7,10-tetraoxa-13-azacyclopentadecane; sodium carbonate; In tetrahydrofuran; diethyl ether; at 20 ℃; for 288h; Overall yield = 53 %; Overall yield = 0.20 g; enantioselective reaction;
DOI:10.1016/j.tetasy.2016.08.010
Guidance literature:
With Methyl-4,6-O-benzylidene-2,3-dideoxy-α-D-glucopyranosido[2,3-h]-N-3-hydroxypropyl-1,4,7,10-tetraoxa-13-azacyclopentadecane; sodium carbonate; In tetrahydrofuran; diethyl ether; at 20 ℃; for 216h; Overall yield = 46 %; Overall yield = 0.19 g; enantioselective reaction;
DOI:10.1016/j.tetasy.2016.08.010
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