phenyl methyl(2-(6-(thiophene-2-carboximidamido)-3,4-dihydroquinolin-1(2H)-yl)ethyl)carbamate

Base Information

Chemical Name:phenyl methyl(2-(6-(thiophene-2-carboximidamido)-3,4-dihydroquinolin-1(2H)-yl)ethyl)carbamate
CAS No.:1063407-57-7
Molecular Formula:C₂₄H₂₆N₄O₂S
Molecular Weight:434.562
Hs Code.:

Synonyms:phenyl methyl(2-(6-(thiophene-2-carboximidamido)-3,4-dihydroquinolin-1(2H)-yl)ethyl)carbamate

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Chemical Property of phenyl methyl(2-(6-(thiophene-2-carboximidamido)-3,4-dihydroquinolin-1(2H)-yl)ethyl)carbamate

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Technology Process of phenyl methyl(2-(6-(thiophene-2-carboximidamido)-3,4-dihydroquinolin-1(2H)-yl)ethyl)carbamate

There total 3 articles about phenyl methyl(2-(6-(thiophene-2-carboximidamido)-3,4-dihydroquinolin-1(2H)-yl)ethyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.2%

: 1063407-55-5
phenyl 2-(6-amino-3,4-dihydroquinolin-1(2H)-yl)ethyl(methyl)carbamate

: methyl thiophene-2-carbimidothioate hydroiodide

: 1063407-57-7
phenyl methyl(2-(6-(thiophene-2-carboximidamido)-3,4-dihydroquinolin-1(2H)-yl)ethyl)carbamate

Guidance literature:: phenyl 2-(6-amino-3,4-dihydroquinolin-1(2H)-yl)ethyl(methyl)carbamate; methyl thiophene-2-carbimidothioate hydroiodide; In ethanol; at 20 ℃;

With water; sodium carbonate; In ethanol; dichloromethane;

Reference yield:

: 1063407-54-4
phenyl methyl(2-(6-nitro-3,4-dihydroquinolin-1(2H)-yl)-ethyl)carbamate

: 1063407-57-7
phenyl methyl(2-(6-(thiophene-2-carboximidamido)-3,4-dihydroquinolin-1(2H)-yl)ethyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen / tetrahydrofuran; ethanol / 4.5 h / Inert atmosphere

2: ethanol / 20 °C / Inert atmosphere

With palladium 10% on activated carbon; hydrogen; In tetrahydrofuran; ethanol;
DOI:10.1021/jm3000449

Reference yield:

: 1885-14-9
phenyl chloroformate

: 1063407-57-7
phenyl methyl(2-(6-(thiophene-2-carboximidamido)-3,4-dihydroquinolin-1(2H)-yl)ethyl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: dichloromethane / 17 h / 20 °C / Inert atmosphere

2: palladium 10% on activated carbon; hydrogen / tetrahydrofuran; ethanol / 4.5 h / Inert atmosphere

3: ethanol / 20 °C / Inert atmosphere

With palladium 10% on activated carbon; hydrogen; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1021/jm3000449