N,N'-bis(2-acetyloxyethyl)-N,N'-bis-1,2-ethanediamine

Base Information

Chemical Name:N,N'-bis(2-acetyloxyethyl)-N,N'-bis-1,2-ethanediamine
CAS No.:238099-16-6
Molecular Formula:C₅₀H₅₈N₄O₁₄
Molecular Weight:939.029
Hs Code.:

N,N'-bis(2-acetyloxyethyl)-N,N'-bis<N'',N''-bis(benzyloxycarbonylmethyl)acetamido>-1,2-ethanediamine

Synonyms:N,N'-bis(2-acetyloxyethyl)-N,N'-bis-1,2-ethanediamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N'-bis(2-acetyloxyethyl)-N,N'-bis-1,2-ethanediamine

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Technology Process of N,N'-bis(2-acetyloxyethyl)-N,N'-bis-1,2-ethanediamine

There total 3 articles about N,N'-bis(2-acetyloxyethyl)-N,N'-bis-1,2-ethanediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 75-36-5
acetyl chloride

: 141996-99-8
N,N-bis(2-hydroxyethyl)-N,N-bis-1,2-ethanediamine

: 238099-16-6
N,N'-bis(2-acetyloxyethyl)-N,N'-bis-1,2-ethanediamine

Guidance literature:: With dmap; In tetrahydrofuran; for 4h; Ambient temperature;
DOI:10.1021/jm980454v

Reference yield:

: 4439-20-7
N,N'-bis(2-hydroxyethyl)ethylene diamine

: 238099-16-6
N,N'-bis(2-acetyloxyethyl)-N,N'-bis-1,2-ethanediamine

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / Et₃N / dimethylformamide / 24 h / 0 °C

2: 50 percent / 4-dimethylaminopyridine / tetrahydrofuran / 4 h / Ambient temperature

With dmap; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jm980454v

Reference yield:

: 137259-44-0
[(bromoacetyl)imino]diacetic acid dibenzyl ester

: 238099-16-6
N,N'-bis(2-acetyloxyethyl)-N,N'-bis-1,2-ethanediamine

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / Et₃N / dimethylformamide / 24 h / 0 °C

2: 50 percent / 4-dimethylaminopyridine / tetrahydrofuran / 4 h / Ambient temperature

With dmap; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jm980454v