2-Chloro-1-iodo-3-methoxybenzene

Base Information

Chemical Name:2-Chloro-1-iodo-3-methoxybenzene
CAS No.:945470-04-2
Molecular Formula:C₇H₆ClIO
Molecular Weight:268.482
Hs Code.:
European Community (EC) Number:969-860-0
Nikkaji Number:J1.866.383J

Synonyms:2-chloro-1-iodo-3-methoxybenzene;945470-04-2;2-chloroiodoanisole;SCHEMBL4619216;KXOUIZYSLOPGME-UHFFFAOYSA-N;DB-192445;F72777;EN300-25683975

Suppliers and Price of 2-Chloro-1-iodo-3-methoxybenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Alichem
2-Chloro-3-iodoanisole
1g
$ 980.00

Total 3 raw suppliers

Chemical Property of 2-Chloro-1-iodo-3-methoxybenzene

Chemical Property:

XLogP3:3.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:267.91519
Heavy Atom Count:10
Complexity:110

Purity/Quality:

98% ^*data from raw suppliers

2-Chloro-3-iodoanisole ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=C(C(=CC=C1)I)Cl

Technology Process of 2-Chloro-1-iodo-3-methoxybenzene

There total 3 articles about 2-Chloro-1-iodo-3-methoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 863870-73-9
O-3-iodophenyl N,N-diethylcarbamate

: 945470-04-2
2-chloro-1-iodo-3-methoxybenzene

Guidance literature:: Multi-step reaction with 3 steps

1.1: LDA / tetrahydrofuran; hexane / 0.5 h / -78 °C

1.2: 70 percent / C₂Cl₆ / tetrahydrofuran; hexane / -78 - 20 °C

2.1: NaOH / ethanol / Heating

3.1: 2.39 g / K₂CO₃ / acetonitrile / Heating

With sodium hydroxide; potassium carbonate; lithium diisopropyl amide; In tetrahydrofuran; ethanol; hexane; acetonitrile;
DOI:10.1021/jo070643y

Reference yield:

: 863870-84-2
O-2-chloro-3-iodophenyl N,N-diethylcarbamate

: 945470-04-2
2-chloro-1-iodo-3-methoxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1: NaOH / ethanol / Heating

2: 2.39 g / K₂CO₃ / acetonitrile / Heating

With sodium hydroxide; potassium carbonate; In ethanol; acetonitrile;
DOI:10.1021/jo070643y