(S)-benzyl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)cyclohex-3-enecarboxylate

Base Information

Chemical Name:(S)-benzyl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)cyclohex-3-enecarboxylate
CAS No.:1449661-86-2
Molecular Formula:C₂₀H₂₇BO₄
Molecular Weight:342.243
Hs Code.:

Synonyms:(S)-benzyl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)cyclohex-3-enecarboxylate

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Chemical Property of (S)-benzyl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)cyclohex-3-enecarboxylate

Chemical Property:

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Technology Process of (S)-benzyl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)cyclohex-3-enecarboxylate

There total 4 articles about (S)-benzyl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)cyclohex-3-enecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1449661-83-9
benzyl 4-(((trifluoromethyl)sulfonyl)oxy)cyclohex-3-enecarboxylate

: 73183-34-3
bis(pinacol)diborane

: 1449661-85-1
(R)-benzyl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)cyclohex-3-enecarboxylate

: 1449661-86-2
(S)-benzyl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)cyclohex-3-enecarboxylate

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; In 1,4-dioxane; at 70 ℃; for 21.5h; Inert atmosphere;

Reference yield:

: 1449661-84-0
benzyl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)cyclohex-3-enecarboxylate

: 1449661-85-1
(R)-benzyl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)cyclohex-3-enecarboxylate

: 1449661-86-2
(S)-benzyl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)cyclohex-3-enecarboxylate

Guidance literature:: Resolution of racemate;

Reference yield:

: 62596-26-3
benzyl 4-oxocyclohexane-1-carboxylate

: 1449661-86-2
(S)-benzyl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)cyclohex-3-enecarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium hexamethylsilazane / tetrahydrofuran / 2.33 h / -78 - 20 °C / Inert atmosphere

2: potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 21.5 h / 70 °C / Inert atmosphere

3: Resolution of racemate

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; potassium hexamethylsilazane; In tetrahydrofuran; 1,4-dioxane;