ω-para methyl cinnamoyl 2-hydroxyacetophenone

Base Information

Chemical Name:ω-para methyl cinnamoyl 2-hydroxyacetophenone
CAS No.:153854-89-8
Molecular Formula:C₁₈H₁₆O₃
Molecular Weight:280.323
Hs Code.:

Synonyms:ω-para methyl cinnamoyl 2-hydroxyacetophenone

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Chemical Property of ω-para methyl cinnamoyl 2-hydroxyacetophenone

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Technology Process of ω-para methyl cinnamoyl 2-hydroxyacetophenone

There total 3 articles about ω-para methyl cinnamoyl 2-hydroxyacetophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 153854-88-7
2-(4-methyl cinnamoyloxy)acetophenone

: 153854-89-8
ω-para methyl cinnamoyl 2-hydroxyacetophenone

Guidance literature:: With potassium hydroxide; In pyridine; at 70 ℃; for 0.25h;
DOI:10.1016/0031-6865(94)90040-X

Reference yield:

: 1866-39-3,940-61-4
trans-p-methylcinnamic acid

: 153854-89-8
ω-para methyl cinnamoyl 2-hydroxyacetophenone

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / SOCl₂ / cyclohexane / 3 h / Heating

2: 97 percent / pyridine / 0.75 h / Ambient temperature

3: 75 percent / KOH / pyridine / 0.25 h / 70 °C

With potassium hydroxide; thionyl chloride; In pyridine; cyclohexane;
DOI:10.1016/0031-6865(94)90040-X

Reference yield:

: 15851-89-5,13565-07-6
(E)-p-methylcinnamoyl chloride

: 153854-89-8
ω-para methyl cinnamoyl 2-hydroxyacetophenone

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / pyridine / 0.75 h / Ambient temperature

2: 75 percent / KOH / pyridine / 0.25 h / 70 °C

With potassium hydroxide; In pyridine;
DOI:10.1016/0031-6865(94)90040-X