(S)-4-methoxy-N-(4-methylpentan-2-yl)aniline

Base Information

Chemical Name:(S)-4-methoxy-N-(4-methylpentan-2-yl)aniline
CAS No.:1073339-61-3
Molecular Formula:C₁₃H₂₁NO
Molecular Weight:207.316
Hs Code.:

Synonyms:(S)-4-methoxy-N-(4-methylpentan-2-yl)aniline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-4-methoxy-N-(4-methylpentan-2-yl)aniline

Chemical Property:

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Technology Process of (S)-4-methoxy-N-(4-methylpentan-2-yl)aniline

There total 7 articles about (S)-4-methoxy-N-(4-methylpentan-2-yl)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 56037-26-4,56037-50-4,61285-48-1
4-methoxy-N-(4-methylpentan-2-ylidene)aniline

: 1073339-61-3
(S)-4-methoxy-N-(4-methylpentan-2-yl)aniline

Guidance literature:: With (R)-3,3'-bis(2,4,6-triisopropylphenyl)binol phosphoric acid; C₈₅H₁₀₂IrN₂O₆PS; hydrogen; In toluene; at 20 ℃; for 15h; under 15001.5 Torr; optical yield given as %ee; enantioselective reaction;
DOI:10.1021/ja807188s

Reference yield:

: 56037-26-4,56037-50-4,61285-48-1
4-methoxy-N-(4-methylpentan-2-ylidene)aniline

: 1073339-61-3
(S)-4-methoxy-N-(4-methylpentan-2-yl)aniline

: 1374002-63-7
(R)-4-methoxy-N-(4-methylpentan-2-yl)aniline

Guidance literature:: 4-methoxy-N-(4-methylpentan-2-ylidene)aniline; With (R)-3,3'-bis(2,4,6-triisopropylphenyl)binol phosphoric acid; In toluene; at 20 ℃; for 0.0833333h; Schlenk technique;

With C₃₅H₅₁IrN₂O₂S; hydrogen; In toluene; at 20 ℃; for 12h; under 15001.5 Torr; Overall yield = 93 %; Optical yield = 58 %ee; enantioselective reaction; Schlenk technique; Autoclave;
DOI:10.1002/chem.201302437

Reference yield:

: 104-94-9
4-methoxy-aniline

: 108-10-1
4-methyl-2-pentanone

: 1073339-61-3
(S)-4-methoxy-N-(4-methylpentan-2-yl)aniline

: 1374002-63-7
(R)-4-methoxy-N-(4-methylpentan-2-yl)aniline

Guidance literature:: With C₈₅H₁₀₂IrN₂O₆PS; hydrogen; In toluene; at 35 ℃; for 12h; under 3750.38 Torr; optical yield given as %ee; enantioselective reaction; Molecular sieve;