1-(Benzyloxy)-4-bromo-2,5-dimethoxybenzene

Base Information

Chemical Name:1-(Benzyloxy)-4-bromo-2,5-dimethoxybenzene
CAS No.:524713-43-7
Molecular Formula:C₁₅H₁₅BrO₃
Molecular Weight:323.186
Hs Code.:
DSSTox Substance ID:DTXSID60453199
Wikidata:Q82274277
Mol file:524713-43-7.mol

Synonyms:1-(Benzyloxy)-4-bromo-2,5-dimethoxybenzene;524713-43-7;1-bromo-2,5-dimethoxy-4-phenylmethoxybenzene;1-Benzyloxy-4-bromo-2,5-dimethoxybenzene;SCHEMBL1318112;DTXSID60453199;GKSZUUGCKYUQMN-UHFFFAOYSA-N;A1-00588

Suppliers and Price of 1-(Benzyloxy)-4-bromo-2,5-dimethoxybenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
1-(Benzyloxy)-4-bromo-2,5-dimethoxybenzene 96%
1g
$ 429.00

Alichem
1-(Benzyloxy)-4-bromo-2,5-dimethoxybenzene
1g
$ 346.50

AccelPharmtech
1-(benzyloxy)-4-bromo-2,5-dimethoxybenzene 97.00%
25G
$ 6000.00

AccelPharmtech
1-(benzyloxy)-4-bromo-2,5-dimethoxybenzene 97.00%
5G
$ 3230.00

Total 3 raw suppliers

Chemical Property of 1-(Benzyloxy)-4-bromo-2,5-dimethoxybenzene

Chemical Property:

Storage Temp.:2-8°C
XLogP3:4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:5
Exact Mass:322.02046
Heavy Atom Count:19
Complexity:256

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

1-(Benzyloxy)-4-bromo-2,5-dimethoxybenzene 96% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC(=C(C=C1OCC2=CC=CC=C2)OC)Br

Technology Process of 1-(Benzyloxy)-4-bromo-2,5-dimethoxybenzene

There total 5 articles about 1-(Benzyloxy)-4-bromo-2,5-dimethoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 74-88-4
methyl iodide

: 524713-43-7
1-benzyloxy-4-bromo-2,5-dimethoxybenzene

Guidance literature:: 5-benzyloxy-2-bromo-4-methoxyphenol; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.333333h;

methyl iodide; In tetrahydrofuran; at 20 ℃; for 18h;

Reference yield: 88.0%

: 524713-42-6
5-benzyloxy-2-bromo-4-methoxyphenol

: 74-88-4
methyl iodide

: 524713-43-7
1-benzyloxy-4-bromo-2,5-dimethoxybenzene

Guidance literature:: 5-benzyloxy-2-bromo-4-methoxyphenol; With sodium hydride; In tetrahydrofuran; for 0.333333h;

methyl iodide; In tetrahydrofuran; at 20 ℃; for 18h;
DOI:10.1021/jm034007d

Reference yield:

: 2973-59-3
2-bromoisovanillin

: 524713-43-7
1-benzyloxy-4-bromo-2,5-dimethoxybenzene

Guidance literature:: Multi-step reaction with 3 steps

1.1: 83 percent / K₂CO₃ / acetonitrile / 20 h / 50 °C

2.1: 85 percent / mCPBA / CH₂Cl₂ / 14 h / Heating

3.1: NaH / tetrahydrofuran / 0.33 h

3.2: 88 percent / tetrahydrofuran / 18 h / 20 °C

With sodium hydride; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1021/jm034007d