N-(2,6-diisopropylphenyl)-N'-(4-iodo-2,6-diisopropylphenyl)ethane-1,2-diamine

Base Information

Chemical Name:N-(2,6-diisopropylphenyl)-N'-(4-iodo-2,6-diisopropylphenyl)ethane-1,2-diamine
CAS No.:1258496-44-4
Molecular Formula:C₂₆H₃₉IN₂
Molecular Weight:506.514
Hs Code.:

Synonyms:N-(2,6-diisopropylphenyl)-N'-(4-iodo-2,6-diisopropylphenyl)ethane-1,2-diamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(2,6-diisopropylphenyl)-N'-(4-iodo-2,6-diisopropylphenyl)ethane-1,2-diamine

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Technology Process of N-(2,6-diisopropylphenyl)-N'-(4-iodo-2,6-diisopropylphenyl)ethane-1,2-diamine

There total 1 articles about N-(2,6-diisopropylphenyl)-N'-(4-iodo-2,6-diisopropylphenyl)ethane-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1189374-17-1
N-(2,6-diisopropylphenyl)-N′-(4-iodo-2,6-diisopropylphenyl)oxalamide

: 1258496-44-4
N-(2,6-diisopropylphenyl)-N'-(4-iodo-2,6-diisopropylphenyl)ethane-1,2-diamine

Guidance literature:: N-(2,6-diisopropylphenyl)-N′-(4-iodo-2,6-diisopropylphenyl)oxalamide; With sodium tetrahydroborate; boron trifluoride diethyl etherate; In tetrahydrofuran; at 20 ℃; for 19h; Reflux;

With hydrogenchloride; water; In tetrahydrofuran; methanol;
DOI:10.1021/om100673e

Reference yield: 90.0%

: 64-17-5
ethanol

: 201230-82-2
carbon monoxide

: 1258496-44-4
N-(2,6-diisopropylphenyl)-N'-(4-iodo-2,6-diisopropylphenyl)ethane-1,2-diamine

: ethyl 4-((2-((2,6-diisopropylphenyl)amino)ethyl)amino)-3,5-diisopropylbenzoate

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; at 110 ℃; for 24h; under 3750.38 Torr; Autoclave;
DOI:10.1002/anie.201600999

Reference yield: 85.0%

: 1258496-44-4
N-(2,6-diisopropylphenyl)-N'-(4-iodo-2,6-diisopropylphenyl)ethane-1,2-diamine

: 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

: 1258496-49-9
C₆H₃(CH(CH₃)2)2NHC₂H₄NHC₆H₂(CH(CH₃)2)2B(OC(CH₃)2)2

Guidance literature:: With K₂CO₃; Et₃N; In 1,4-dioxane; B compd. and Et3N were added to suspn. of diamine and Pd complex in dioxane; heated at 80°C for 12 h; H2O added; extd. (Et2O); org. layer dried (MgSO4); concd.; chromd. (silica gel, hexane/EtOAc, 25/1); elem. anal.;
DOI:10.1021/om100673e