N-[2-[1-(2,3-dimethoxyphenyl)]-ethyl]2-bromo-3,4-dimethoxyphenylacetamide

Base Information

Chemical Name:N-[2-[1-(2,3-dimethoxyphenyl)]-ethyl]2-bromo-3,4-dimethoxyphenylacetamide
CAS No.:1254068-23-9
Molecular Formula:C₂₀H₂₄BrNO₅
Molecular Weight:438.318
Hs Code.:

Synonyms:N-[2-[1-(2,3-dimethoxyphenyl)]-ethyl]2-bromo-3,4-dimethoxyphenylacetamide

Suppliers and Price of N-[2-[1-(2,3-dimethoxyphenyl)]-ethyl]2-bromo-3,4-dimethoxyphenylacetamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-[2-[1-(2,3-dimethoxyphenyl)]-ethyl]2-bromo-3,4-dimethoxyphenylacetamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-[2-[1-(2,3-dimethoxyphenyl)]-ethyl]2-bromo-3,4-dimethoxyphenylacetamide

There total 5 articles about N-[2-[1-(2,3-dimethoxyphenyl)]-ethyl]2-bromo-3,4-dimethoxyphenylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 3213-29-4
2,3-dimethoxyphenethylamine

: 104421-97-8
2-bromo-3,4-dimethoxyphenylacetyl chloride

: 1254068-23-9
N-[2-[1-(2,3-dimethoxyphenyl)]-ethyl]2-bromo-3,4-dimethoxyphenylacetamide

Guidance literature:: With sodium carbonate; In chloroform; at 0 ℃; Inert atmosphere;

Reference yield:

: 72912-38-0
(2-bromo-3,4-dimethoxyphenyl)methanol

: 1254068-23-9
N-[2-[1-(2,3-dimethoxyphenyl)]-ethyl]2-bromo-3,4-dimethoxyphenylacetamide

Guidance literature:: Multi-step reaction with 5 steps

1: hydrogenchloride / toluene

2: dimethyl sulfoxide

3: sulfuric acid; water; acetic acid

4: oxalyl dichloride / dichloromethane / 2 h

5: sodium carbonate / chloroform / 0 °C / Inert atmosphere

With hydrogenchloride; oxalyl dichloride; sulfuric acid; water; sodium carbonate; acetic acid; In dichloromethane; chloroform; dimethyl sulfoxide; toluene;
DOI:10.1016/j.bmcl.2012.08.123

Reference yield:

: 63856-83-7
2-bromo-3,4-dimethoxyphenylacetic acid

: 1254068-23-9
N-[2-[1-(2,3-dimethoxyphenyl)]-ethyl]2-bromo-3,4-dimethoxyphenylacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl dichloride / dichloromethane / 2 h

2: sodium carbonate / chloroform / 0 °C / Inert atmosphere

With oxalyl dichloride; sodium carbonate; In dichloromethane; chloroform;
DOI:10.1016/j.bmcl.2012.08.123