C₂₇H₃₃NO₆S

Base Information

Chemical Name:C₂₇H₃₃NO₆S
CAS No.:478490-11-8
Molecular Formula:C₂₇H₃₃NO₆S
Molecular Weight:499.628
Hs Code.:

C<sub>27</sub>H<sub>33</sub>NO<sub>6</sub>S

Synonyms:C₂₇H₃₃NO₆S

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Chemical Property of C₂₇H₃₃NO₆S

Chemical Property:

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Technology Process of C₂₇H₃₃NO₆S

There total 10 articles about C₂₇H₃₃NO₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 98-09-9
benzenesulfonyl chloride

: 478490-10-7
C₂₁H₂₉NO₄

: 478490-11-8
C₂₇H₃₃NO₆S

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1021/ol027040n

Reference yield:

: 89980-69-8
3,4-dimethoxyphenylmagnesium bromide

: 478490-11-8
C₂₇H₃₃NO₆S

Guidance literature:: Multi-step reaction with 5 steps

1: CuBr*Me₂S / hexamethylphosphoric acid triamide; tetrahydrofuran / -78 °C

2: tetrabutylammonium fluoride

3: 77 percent / p-toluenesulfonic acid / toluene / Heating

4: 95 percent / lithium aluminum hydride / tetrahydrofuran / Heating

5: 82 percent / triethylamine / CH₂Cl₂ / 0 - 20 °C

With lithium aluminium tetrahydride; copper(I) bromide dimethylsulfide complex; tetrabutyl ammonium fluoride; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane; toluene;
DOI:10.1021/ol027040n

Reference yield:

: 351033-77-7
(1S,5S,6S)-6-Methoxymethoxy-bicyclo[3.2.1]oct-3-en-2-one

: 478490-11-8
C₂₇H₃₃NO₆S

Guidance literature:: Multi-step reaction with 9 steps

1: 92 percent / butyllithium / tetrahydrofuran / -78 °C

2: lithium aluminum hydride / tetrahydrofuran

3: triethylamine / CH₂Cl₂

4: 89 percent / pyridinium chlorochromate / CH₂Cl₂

5: CuBr*Me₂S / hexamethylphosphoric acid triamide; tetrahydrofuran / -78 °C

6: tetrabutylammonium fluoride

7: 77 percent / p-toluenesulfonic acid / toluene / Heating

8: 95 percent / lithium aluminum hydride / tetrahydrofuran / Heating

9: 82 percent / triethylamine / CH₂Cl₂ / 0 - 20 °C

With lithium aluminium tetrahydride; n-butyllithium; copper(I) bromide dimethylsulfide complex; tetrabutyl ammonium fluoride; toluene-4-sulfonic acid; triethylamine; pyridinium chlorochromate; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane; toluene;
DOI:10.1021/ol027040n