1-[N-(2,6-dimethylphenyl)-N-(ethoxycarbonyl)-amino]-2-dimethylamino-propan

Base Information

Chemical Name:1-[N-(2,6-dimethylphenyl)-N-(ethoxycarbonyl)-amino]-2-dimethylamino-propan
CAS No.:83843-86-1
Molecular Formula:C₁₆H₂₆N₂O₂
Molecular Weight:278.395
Hs Code.:

Synonyms:1-[N-(2,6-dimethylphenyl)-N-(ethoxycarbonyl)-amino]-2-dimethylamino-propan

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Chemical Property of 1-[N-(2,6-dimethylphenyl)-N-(ethoxycarbonyl)-amino]-2-dimethylamino-propan

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Technology Process of 1-[N-(2,6-dimethylphenyl)-N-(ethoxycarbonyl)-amino]-2-dimethylamino-propan

There total 6 articles about 1-[N-(2,6-dimethylphenyl)-N-(ethoxycarbonyl)-amino]-2-dimethylamino-propan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 541-41-3
chloroformic acid ethyl ester

: 83843-49-6
1-(2,6-Dimethyl-Phenyl-amino)-2-Dimethyl-amino-Propane

: 83843-86-1
1-[N-(2,6-dimethylphenyl)-N-(ethoxycarbonyl)-amino]-2-dimethylamino-propan

Guidance literature:: With triethylamine; In 1,2-dichloro-ethane; for 5h; Heating;

Reference yield:

: 66236-09-7
N-(2,6-dimethylphenyl)-methane sulfonamide

: 83843-86-1
1-[N-(2,6-dimethylphenyl)-N-(ethoxycarbonyl)-amino]-2-dimethylamino-propan

Guidance literature:: Multi-step reaction with 5 steps

1: 70 percent / 0.5N NaOH / 1) 80 - 85 deg C, 4 h, 2) RT, overnight

2: 88 percent / pyridine / 3 h / 0 - 5 °C

3: 83 percent / ethanol / 120 - 125 °C / steel bomb

4: 89 percent / liq. NH₃, Na / toluene; propan-2-ol / 2 h / -40 - -35 °C

5: 67 percent / Et₃N / 1,2-dichloro-ethane / 5 h / Heating

With pyridine; sodium hydroxide; ammonia; sodium; triethylamine; In ethanol; 1,2-dichloro-ethane; isopropyl alcohol; toluene;

Reference yield:

: 87-62-7
2,6-dimethylaniline

: 83843-86-1
1-[N-(2,6-dimethylphenyl)-N-(ethoxycarbonyl)-amino]-2-dimethylamino-propan

Guidance literature:: Multi-step reaction with 6 steps

1: 91 percent

2: 70 percent / 0.5N NaOH / 1) 80 - 85 deg C, 4 h, 2) RT, overnight

3: 88 percent / pyridine / 3 h / 0 - 5 °C

4: 83 percent / ethanol / 120 - 125 °C / steel bomb

5: 89 percent / liq. NH₃, Na / toluene; propan-2-ol / 2 h / -40 - -35 °C

6: 67 percent / Et₃N / 1,2-dichloro-ethane / 5 h / Heating

With pyridine; sodium hydroxide; ammonia; sodium; triethylamine; In ethanol; 1,2-dichloro-ethane; isopropyl alcohol; toluene;